Organic Analytical Service Target Analytes
Volatiles
| ANALYTE | CAS No. | SOM02.4 CONTRACT REQUIRED QUANTITATION LIMITS | ||||
|---|---|---|---|---|---|---|
| Trace Water (ug/L) |
Low Water (ug/L) |
Low Soil (ug/kg) |
Med. Soil (ug/kg) |
TCLP (mg/L) |
||
| Dichlorodifluoromethane | 75-71-8 | 0.50 | 5.0 | 5.0 | 250 | |
| Chloromethane | 74-87-3 | 0.50 | 5.0 | 5.0 | 250 | |
| Vinyl chloride | 75-01-4 | 0.50 | 5.0 | 5.0 | 250 | 0.0050 |
| Bromomethane | 74-83-9 | 0.50 | 5.0 | 5.0 | 250 | |
| Chloroethane | 75-00-3 | 0.50 | 5.0 | 5.0 | 250 | |
| Trichlorofluoromethane | 75-69-4 | 0.50 | 5.0 | 5.0 | 250 | |
| 1,1-Dichloroethene | 75-35-4 | 0.50 | 5.0 | 5.0 | 250 | 0.0050 |
| 1,1,2-Trichloro-1,2,2-trifluoroethane | 76-13-1 | 0.50 | 5.0 | 5.0 | 250 | |
| Acetone | 67-64-1 | 5.0 | 10 | 10 | 500 | |
| Carbon disulfide | 75-15-0 | 0.50 | 5.0 | 5.0 | 250 | |
| Methyl acetate | 79-20-9 | 0.50 | 5.0 | 5.0 | 250 | |
| Methylene chloride | 75-09-2 | 0.50 | 5.0 | 5.0 | 250 | |
| trans-1,2-Dichloroethene | 156-60-5 | 0.50 | 5.0 | 5.0 | 250 | |
| Methyl tert-butyl ether | 1634-04-4 | 0.50 | 5.0 | 5.0 | 250 | |
| 1,1-Dichloroethane | 75-34-3 | 0.50 | 5.0 | 5.0 | 250 | |
| cis-1,2-Dichloroethene | 156-59-2 | 0.50 | 5.0 | 5.0 | 250 | |
| 2-Butanone | 78-93-3 | 5.0 | 10 | 10 | 500 | 0.010 |
| Bromochloromethane | 74-97-5 | 0.50 | 5.0 | 5.0 | 250 | |
| Chloroform | 67-66-3 | 0.50 | 5.0 | 5.0 | 250 | 0.0050 |
| 1,1,1-Trichloroethane | 71-55-6 | 0.50 | 5.0 | 5.0 | 250 | |
| Cyclohexane | 110-82-7 | 0.50 | 5.0 | 5.0 | 250 | |
| Carbon tetrachloride | 56-23-5 | 0.50 | 5.0 | 5.0 | 250 | 0.0050 |
| Benzene | 71-43-2 | 0.50 | 5.0 | 5.0 | 250 | 0.0050 |
| 1,2-Dichloroethane | 107-06-2 | 0.50 | 5.0 | 5.0 | 250 | 0.0050 |
| Trichloroethene | 79-01-6 | 0.50 | 5.0 | 5.0 | 250 | 0.0050 |
| Methylcyclohexane | 108-87-2 | 0.50 | 5.0 | 5.0 | 250 | |
| 1,2-Dichloropropane | 78-87-5 | 0.50 | 5.0 | 5.0 | 250 | |
| Bromodichloromethane | 75-27-4 | 0.50 | 5.0 | 5.0 | 250 | |
| cis-1,3-Dichloropropene | 10061-01-5 | 0.50 | 5.0 | 5.0 | 250 | |
| 4-Methyl-2-pentanone | 108-10-1 | 5.0 | 10 | 10 | 500 | |
| Toluene | 108-88-3 | 0.50 | 5.0 | 5.0 | 250 | |
| trans-1,3-Dichloropropene | 10061-02-6 | 0.50 | 5.0 | 5.0 | 250 | |
| 1,1,2-Trichloroethane | 79-00-5 | 0.50 | 5.0 | 5.0 | 250 | |
| Tetrachloroethene | 127-18-4 | 0.50 | 5.0 | 5.0 | 250 | 0.0050 |
| 2-Hexanone | 591-78-6 | 5.0 | 10 | 10 | 500 | |
| Dibromochloromethane | 124-48-1 | 0.50 | 5.0 | 5.0 | 250 | |
| 1,2-Dibromoethane | 106-93-4 | 0.50 | 5.0 | 5.0 | 250 | |
| Chlorobenzene | 108-90-7 | 0.50 | 5.0 | 5.0 | 250 | 0.0050 |
| Ethylbenzene | 100-41-4 | 0.50 | 5.0 | 5.0 | 250 | |
| o-Xylene | 95-47-6 | 0.50 | 5.0 | 5.0 | 250 | |
| m,p-Xylene | 179601-23-1 | 0.50 | 5.0 | 5.0 | 250 | |
| Styrene | 100-42-5 | 0.50 | 5.0 | 5.0 | 250 | |
| Bromoform | 75-25-2 | 0.50 | 5.0 | 5.0 | 250 | |
| Isopropylbenzene | 98-82-8 | 0.50 | 5.0 | 5.0 | 250 | |
| 1,1,2,2-Tetrachloroethane | 79-34-5 | 0.50 | 5.0 | 5.0 | 250 | |
| 1,3-Dichlorobenzene | 541-73-1 | 0.50 | 5.0 | 5.0 | 250 | |
| 1,4-Dichlorobenzene | 106-46-7 | 0.50 | 5.0 | 5.0 | 250 | 0.0050 |
| 1,2-Dichlorobenzene | 95-50-1 | 0.50 | 5.0 | 5.0 | 250 | |
| 1,2-Dibromo-3-chloropropane | 96-12-8 | 0.50 | 5.0 | 5.0 | 250 | |
| 1,2,4-Trichlorobenzene | 120-82-1 | 0.50 | 5.0 | 5.0 | 250 | |
| 1,2,3-Trichlorobenzene | 87-61-6 | 0.50 | 5.0 | 5.0 | 250 | |
Semivolatiles
| ANALYTE | CAS No. | SOM02.4 CONTRACT REQUIRED QUANTITATION LIMITS | |||||
|---|---|---|---|---|---|---|---|
| Low Water by SIM (ug/L) |
Low Water (ug/L) |
Low Soil by SIM (ug/kg) |
Low Soil (ug/kg) |
Med. Soil (ug/kg) |
TCLP (mg/L) |
||
| 1.4-Dioxane | 123-91-1 | -- | 2.0 | -- | 67 | 2,000 | |
| Benzaldehyde | 100-52-7 | -- | 10 | -- | 330 | 10,000 | |
| Phenol | 108-95-2 | -- | 10 | -- | 330 | 10,000 | |
| Bis(2-chloroethyl) ether | 111-44-4 | -- | 10 | -- | 330 | 10,000 | |
| 2-Chlorophenol | 95-57-8 | -- | 5.0 | -- | 170 | 5,000 | |
| 2-Methylphenol | 95-48-7 | -- | 10 | -- | 330 | 10,000 | 0.010 |
| 3-Methylphenol1 | 108-39-4 | -- | 5.0 | -- | -- | -- | 0.0050 |
| 2,2'-Oxybis(1-choloropropane) | 108-60-1 | -- | 10 | -- | 330 | 10,000 | |
| Acetophenone | 98-86-2 | -- | 10 | -- | 330 | 10,000 | |
| 4-Methylphenol1 | 106-44-5 | -- | 10 | -- | 330 | 10,000 | 0.010 |
| N-Nitroso-di-n propylamine | 621-64-7 | -- | 5.0 | -- | 170 | 5,000 | |
| Hexachloroethane | 67-72-1 | -- | 5.0 | -- | 170 | 5,000 | 0.0050 |
| Nitrobenzene | 98-95-3 | -- | 5.0 | -- | 170 | 5,000 | 0.0050 |
| Isophorone | 78-59-1 | -- | 5.0 | -- | 170 | 5,000 | |
| 2-Nitrophenol | 88-75-5 | -- | 5.0 | -- | 170 | 5,000 | |
| 2,4-Dimethylphenol | 105-67-9 | -- | 5.0 | -- | 170 | 5,000 | |
| Bis(2-chloroethoxy) methane | 111-91-1 | -- | 5.0 | -- | 170 | 5,000 | |
| 2,4-Dichlorophenol | 120-83-2 | -- | 5.0 | -- | 170 | 5,000 | |
| Naphthalene | 91-20-3 | 0.10 | 5.0 | 3.3 | 170 | 5,000 | |
| 4-Chloroaniline | 106-47-8 | -- | 10 | -- | 330 | 10,000 | |
| Hexachlorobutadiene | 87-68-3 | -- | 5.0 | -- | 170 | 5,000 | 0.0050 |
| Caprolactam | 105-60-2 | -- | 10 | -- | 330 | 10,000 | |
| 4-Chloro-3-methylphenol | 59-50-7 | -- | 5.0 | -- | 170 | 5,000 | |
| 2-Methylnaphthalene | 91-57-6 | 0.10 | 5.0 | 3.3 | 170 | 5,000 | |
| Hexachlorocyclopentadiene | 77-47-4 | -- | 10 | -- | 330 | 10,000 | |
| 2,4,6-Trichlorophenol | 88-06-2 | -- | 5.0 | -- | 170 | 5,000 | 0.0050 |
| 2,4,5-Trichlorophenol | 95-95-4 | -- | 5.0 | -- | 170 | 5,000 | 0.0050 |
| 1,1'-Biphenyl | 92-52-4 | -- | 5.0 | -- | 170 | 5,000 | |
| 2-Chloronaphthalene | 91-58-7 | -- | 5.0 | -- | 170 | 5,000 | |
| 2-Nitroaniline | 88-74-4 | -- | 5.0 | -- | 170 | 5,000 | |
| Dimethylphthalate | 131-11-3 | -- | 5.0 | -- | 170 | 5,000 | |
| 2,6-Dinitrotoluene | 606-20-2 | -- | 5.0 | -- | 170 | 5,000 | |
| Acenaphthylene | 208-96-8 | 0.10 | 5.0 | 3.3 | 170 | 5,000 | |
| 3-Nitroaniline | 99-09-2 | -- | 10 | -- | 330 | 10,000 | |
| Acenaphthene | 83-32-9 | 0.10 | 5.0 | 3.3 | 170 | 5,000 | |
| 2,4-Dinitrophenol | 51-28-5 | -- | 10 | -- | 330 | 10,000 | |
| 4-Nitrophenol | 100-02-7 | -- | 10 | -- | 330 | 10,000 | |
| Dibenzofuran | 132-64-9 | -- | 5.0 | -- | 170 | 5,000 | |
| 2,4-Dinitrotoluene | 121-14-2 | -- | 5.0 | -- | 170 | 5,000 | 0.0050 |
| Diethylphthalate | 84-66-2 | -- | 5.0 | -- | 170 | 5,000 | |
| Fluorene | 86-73-7 | 0.10 | 5.0 | 3.3 | 170 | 5,000 | |
| 4-Chlorophenyl-phenyl ether | 7005-72-3 | -- | 5.0 | -- | 170 | 5,000 | |
| 4-Nitroaniline | 100-01-6 | -- | 10 | -- | 330 | 10,000 | |
| 4,6-Dinitro-2-methylphenol | 534-52-1 | -- | 10 | -- | 330 | 10,000 | |
| N-Nitrosodiphenylamine | 86-30-6 | -- | 5.0 | -- | 170 | 5,000 | |
| 1,2,4,5-Tetrachlorobenzene | 95-94-3 | -- | 5.0 | -- | 170 | 5,000 | |
| 4-Bromophenyl-phenylether | 101-55-3 | -- | 5.0 | -- | 170 | 5,000 | |
| Hexachlorobenzene | 118-74-1 | -- | 5.0 | -- | 170 | 5,000 | 0.0050 |
| Atrazine | 1912-24-9 | -- | 10 | -- | 330 | 10,000 | |
| Pentachlorophenol | 87-86-5 | 0.20 | 10 | 6.7 | 330 | 10,000 | 0.010 |
| Phenanthrene | 85-01-8 | 0.10 | 5.0 | 3.3 | 170 | 5,000 | 0.0050 |
| Anthracene | 120-12-7 | 0.10 | 5.0 | 3.3 | 170 | 5,000 | |
| Carbazole | 86-74-8 | -- | 10 | -- | 330 | 10,000 | |
| Di-n-butylphthalate | 84-74-2 | -- | 5.0 | -- | 170 | 5,000 | |
| Fluoranthene | 206-44-0 | 0.10 | 10 | 3.3 | 330 | 10,000 | |
| Pyrene | 129-00-0 | 0.10 | 5.0 | 3.3 | 170 | 5,000 | |
| Butylbenzylphthalate | 85-68-7 | -- | 5.0 | -- | 170 | 5,000 | |
| 3,3'-Dicholorobenzidine | 91-94-1 | -- | 10 | -- | 330 | 10,000 | |
| Benzo(a)anthracene | 56-55-3 | 0.10 | 5.0 | 3.3 | 170 | 5,000 | |
| Chrysene | 218-01-9 | 0.10 | 5.0 | 3.3 | 170 | 5,000 | |
| Bis(2-ethylhexyl) phthalate | 117-81-7 | -- | 5.0 | -- | 170 | 5,000 | |
| Di-n-octylphthalate | 117-84-0 | -- | 10 | -- | 330 | 10,000 | |
| Benzo(b) fluoranthene | 205-99-2 | 0.10 | 5.0 | 3.3 | 170 | 5,000 | |
| Benzo(k) fluoranthene | 207-08-9 | 0.10 | 5.0 | 3.3 | 170 | 5,000 | |
| Benzo(a) pyrene | 50-32-8 | 0.10 | 5.0 | 3.3 | 170 | 5,000 | |
| Indeno(1,2,3,-cd) pyrene | 193-39-5 | 0.10 | 5.0 | 3.3 | 170 | 5,000 | |
| Dibenzo(a,h) anthracene | 53-70-3 | 0.10 | 5.0 | 3.3 | 170 | 5,000 | |
| Benzo(g,h,i) perylene | 191-24-2 | 0.10 | 5.0 | 3.3 | 170 | 5,000 | |
| 2,3,4,6-Tetrachlorophenol | 58-90-2 | -- | 5.0 | -- | 170 | 5,000 | |
1 Semivolatile target analyte 3-methylphenol is included in this table ONLY for inclusion in the list of TCLP and/or SPLP analytes. Compounds 3-Methylphenol and 4-Methylphenol cannot be separated by the extraction techniques or GC columns used in this method. Therefore, both are represented in this SOW by the 4-methylphenol isomer only. Those data users who wish to analyze 3- and 4-methylphenol separately are encouraged to utilize the CLP-MA process to obtain data for these compounds from the derivatization/GC method (8041A or equivalent).
Pesticides and Aroclors
| ANALYTE | CAS No. | SOM02.4 CONTRACT REQUIRED QUANTITATION LIMITS |
||
|---|---|---|---|---|
| Water (ug/L) |
Soil (ug/Kg) |
TCLP (mg/L) |
||
| alpha-BHC | 319-84-6 | 0.050 | 1.7 | |
| beta-BHC | 319-85-7 | 0.050 | 1.7 | |
| delta-BHC | 319-86-8 | 0.050 | 1.7 | |
| gamma-BHC (Lindane) | 58-89-9 | 0.050 | 1.7 | 0.000050 |
| Heptachlor | 76-44-8 | 0.050 | 1.7 | 0.000050 |
| Aldrin | 309-00-2 | 0.050 | 1.7 | |
| Heptachlor epoxide | 1024-57-3 | 0.050 | 1.7 | 0.000050 |
| Endosulfan I | 959-98-8 | 0.050 | 1.7 | |
| Dieldrin | 60-57-1 | 0.10 | 3.3 | |
| 4,4'-DDE | 72-55-9 | 0.10 | 3.3 | |
| Endrin | 72-20-8 | 0.10 | 3.3 | 0.00010 |
| Endosulfan II | 33213-65-9 | 0.10 | 3.3 | |
| 4,4'-DDD | 72-54-8 | 0.10 | 3.3 | |
| Endosulfan sulfate | 1031-07-8 | 0.10 | 3.3 | |
| 4,4'-DDT | 50-29-3 | 0.10 | 3.3 | |
| Methoxychlor | 72-43-5 | 0.50 | 17.0 | 0.00050 |
| Endrin ketone | 53494-70-5 | 0.10 | 3.3 | |
| Endrin aldehyde | 7421-93-4 | 0.10 | 3.3 | |
| cis-Chlordane | 5103-71-9 | 0.050 | 1.7 | 0.000050 |
| trans-Chlordane | 5103-74-2 | 0.050 | 1.7 | 0.000050 |
| Toxaphene | 8001-35-2 | 5.0 | 170 | 0.0050 |
| Aroclor-1016 | 12674-11-2 | 1.0 | 33.0 | |
| Aroclor-1221 | 11104-28-2 | 1.0 | 33.0 | |
| Aroclor-1232 | 11141-16-5 | 1.0 | 33.0 | |
| Aroclor-1242 | 53469-21-9 | 1.0 | 33.0 | |
| Aroclor-1248 | 12672-29-6 | 1.0 | 33.0 | |
| Aroclor-1254 | 11097-69-1 | 1.0 | 33.0 | |
| Aroclor-1260 | 11096-82-5 | 1.0 | 33.0 | |
| Aroclor-1262 | 37324-23-5 | 1.0 | 33.0 | |
| Aroclor-1268 | 11100-14-4 | 1.0 | 33.0 | |