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Basic Information about How to Use SW-846

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What is SW-846?

The Test Methods for Evaluating Solid Waste: Physical/Chemical Methods Compendium, also known as SW-846 or the Compendium, is EPA’s official collection of methods for use in complying with the Resource Conservation and Recovery Act (RCRA) regulations. SW-846 is organized into chapters providing guidance on how to use the methods and groups of methods, called “series”, which are organized by topic. The methods and chapters change over time as updates are published to keep up with evolving analytical and measurement needs.

In addition to the methods that are in the official SW-846 compendium, EPA has validated methods. These methods are tested and validated by laboratories and go through extensive review, but they have not been incorporated into SW-846 through the Federal Register process. EPA encourages using the validated methods, if possible, for the most current version of a method. 

For more information on how to use the SW-846 Compendium and related documents, please view our collection of frequent questions

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Which Method Should I Use?

Chapter 2 of SW-846 provides general guidance on the important aspects of choosing an analytical method. This chapter also contains more detailed information on the appropriate methods for specific analytes.

Additionally, the interactive table below can be used to find methods by number, analyte, Chemical Abstracts Service (CAS) number, analytical technique, or matrix. Type your search terms into the search box or sort the categories by alphabet. The table includes a listing of all SW-846 Test Method documents along with details on each method a link to the method's PDF document.

Please note that validated methods are not included in this table. 

Method # Title Type Analyte CAS # Technique Media/Matrix Date
#0010 Modified Method 5 Sampling Train sampling semivolatile principal organic hazardous compounds (POHCs) NA isokinetic sampling train emissions Sept. 1986
#0011 Sampling for Selected Aldehyde and Ketone Emissions from Stationary Sources sampling formaldehyde, acetaldehyde,isophorone, propionaldehyde, other aldehydes and ketones 50-00-0, 75-07-0, 98-86-2, 78-59-1, 123-38-6 isokinetic extraction emissions Dec. 1996
#0020 Source Assessment Sampling System (SASS) sampling particulate and semivolatile organic materials NA isokinetic sampling train particulates, emissions Sept. 1986
#0023A Sampling Method for Polychlorinated Dibenzo-p-Dioxins and Polychlorinated Dibenzofuran Emissions from Stationary Sources sampling polychlorinated dibenzo-p-dioxins (PCDDs), polychlorinated dibenzofurans (PCDFs) NA isokinetic sampling train emissions Dec. 1996
#0030 Volatile Organic Sampling Train sampling volatile principal organic hazardous constituents (POHCs) NA sampling train emissions Sept. 1986
#0031 Sampling Method for Volatile Organic Compounds (SMVOC) sampling volatile organic compounds (VOCs) with a boiling point between -15°C and 121°C: acrylonitrile, benzene, bromodichloromethane, carbon disulfide, carbon tetrachloride, chlorodibromomethane, 1,1-dichloroethane, 1,2-dichlororethane, 1,1-dichloroethene, trans-1,2-dichloroethene, 1,2-dichloropropane, 1,3-dichloropropene, methylene chloride, tetrachloroethene, toluene, 1,1,1-trichloroethane, 1,1,2-trichloroethane, trichloroethene, trichlorofluoromethane 107-13-1, 71-43-2, 75-27-4, 75-15-0, 56-23-5, 124-48-1, 67-66-3, 126-99-8, 74-95-3, 75-34-3, 107-06-2, 75-35-4, 156-60-5, 78-87-5, 542-75-6, 75-09-2, 127-18-4, 108-88-3, 71-55-6, 79-00-5, 79-01-6, 75-69-4 sampling train emissions Dec. 1996
#0040 Sampling of Principle Organic Hazardous Constituents from Combustion Sources Using Tedlar® Bags sampling volatile organic compounds (VOCs): 1,1,1-trichloroethane, trichloroethene, 1,1-dichloroethane, 1,1-dichloroethene, 2,2,4-trimethylpentane, allyl chloride, benzene, carbon tetrachloride, methyl chloride, n-hexane, methylene chloride, toluene, trichlorofluoromethane, vinyl bromide, vinyl chloride, methyl bromide, 1,3-butadiene, dichlorofluoromethane, 1,2-dichloro-1,1,2,2-tetrafluoroethane, 1,1,2-trichlorotrifluoroethane, chloroform, 1,2-dichloropropane, tetrachloroethene 71-55-6, 79-01-6, 75-34-3, 75-35-4, 540-84-1, 107-05-1, 71-43-2, 56-23-5, 74-87-3, 110-54-3, 75-09-2, 108-88-3, 353-54-8, 593-60-2, 75-01-4, 74-83-9, 106-99-0, 75-71-8, 76-14-2, 76-13-1, 67-66-3, 78-87-5, 127-18-4 time-integrated evacuated Tedlar® bags emissions Dec. 1996
#0050 Isokinetic HCl/Cl2 Emission Sampling Train sampling hydrogen chloride (HCl), chlorine (Cl2) 7647-01-0, 7782-50-5 isokinetic sampling train emissions Dec. 1996
#0051 Midget Impinger HCl/Cl2 Emission Sampling Train sampling hydrogen chloride (HCl), chlorine (Cl2) 7647-01-0, 7782-50-5 midget impinger sampling train emissions Dec. 1996
#0060 Determination of Metals in Stack Emissions sampling metals: antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), cadmium (Cd), chromium (Cr), cobalt (Co), copper (Cu), lead (Pb), manganese (Mn), mercury (Hg), nickel (Ni), phosphorus (P), selenium (Se), silver (Ag), thallium (Tl), zinc (Zn) 7440-36-0, 7440-38-2, 7440-39-3, 7440-41-7, 7440-43-9, 7440-47-3, 7440-48-4, 7440-50-8, 7439-92-1, 7439-96-5, 7439-97-6, 7440-02-0, 7803-51-2, 7782-49-2, 7440-22-4, 7440-28-0, 7440-66-6 isokinetic chilled impinger sampling train emissions Dec. 1996
#0061 Determination of Hexavalent Chromium Emissions from Stationary Sources sampling hexavalent chromium (Cr6+) 18540-29-9 Isokinetic sampling train emissions Dec. 1996
#0100 Sampling for Formaldehyde and Other Carbonyl Compounds in Indoor Air sampling Carbonyl Compounds: acetaldehyde, acetone, acrolein, benzaldehyde, butyraldehyde, crotonaldehyde, 2,5-dimethylbenzaldehyde, formaldehyde, hexanal, isovaleraldehyde, propionaldehyde, m-tolualdehyde, o-tolualdehyde, p-tolualdehyde, valeraldehyde 75-07-0, 67-64-1, 107-02-8, 100-52-7, 123-72-8, 123-73-9, 5779-94-2, 50-00-0, 66-25-1, 590-86-3, 123-38-6, 620-23-5, 529-20-4, 104-87-0, 110-62-3 Derivatization with 2,4-dinitrophenylhydrazine (DNPH) indoor air Dec. 1996
25D Determination of the Volatile Organic Concentration of Waste Samples determinative volatile organic compounds (VOCs) NA flame ionization detector (FID), electrolytic conductivity detector (ELCD) air waste Feb. 2007
25E Determination of Vapor Phase Organic Concentration in Waste Samples determinative vapor phase organic compounds NA headspace analyzer, flame ionization detector (FID) air waste Feb. 2007
207/OTM 14 Method for Measuring Isocyanates determinative isocyanates: 2,4-toluene diisocyanate (TDI), 1,6-hexamethylene diisocyanate (HDI), methylene diphenyl diisocyanate (MDI), methyl isocyanate (MI) 584-84-9, 822-06-0, 101-68-8, 624-83-9 isokinetic sampling train, high performance liquid chromatography (HPLC) emissions Feb. 2007
1010A Test Methods for Flash Point by Pensky-Martens Closed-Cup Tester characterization flashpoint NA Pensky-Martens Closed-Cup Tester petroleum products, biodiesel Nov. 2004
1020B Standard Test Methods for Flash Point by Setaflash (Small Scale) Closed-Cup Apparatus characterization flashpoint NA small scale closed-cup apparatus paints, enamels, lacquers, varnishes, other products with a flash point between 0°C and 110°C Nov. 2004
1030 Ignitability of Solids Characterization ignitability NA combustion pastes, granular materials, strips, powders July 2014
1040 Test Method for Oxidizing Solids characterization oxidizing hazard NA conical pile-type burning solids, granular materials Feb. 2007
1050 Test Methods to Determine Substances Likely to Spontaneously Combust characterization spontaneous combustion NA pryophoric classification tests liquid waste, solid waste Feb. 2007
1110A Corrosivity Toward Steel characterization corrosivity NA steel exposure aqueous waste, non-aqueous liquid waste Nov. 2004
1120 Dermal Corrosion characterization corrosivity to skin NA in vitro test method solids, liquids, and emulsions Dec. 1996
1310B Extraction Procedure (EP) Toxicity Test Method and Structural Integrity Test characterization extraction procedure toxicity, structural integrity NA extraction, structural integrity test Liquids, solids, multiphase samples Nov. 2004
1311 Toxicity Characteristic Leaching Procedure (TCLP) characterization toxicity characteristic NA extraction Liquids, solids, multiphase wastes July 1992
1312 Synthetic Precipitation Leaching Procedure (SPLP) characterization mobility of organic and inorganic compounds NA synthetic precipitation liquids, soils, wastes July 1992
1313 Liquid-Solid Partitioning as a Function of Extract pH Using a Parallel Batch Extraction Procedure characterization leaching of inorganic compounds NA batch extraction solid materials July 2017
1314 Liquid-Solid Partitioning as a Function of Liquid-Solid Ratio for Constituents in Solid Materials Using an Up-Flow Percolation Column Procedure characterization leaching of inorganic compounds NA up-flow percolation column granular solid materials July 2017
1315 Mass Transfer Rates of Constituents in Monolithic or Compacted Granular Materials Using a Semi-Dynamic Tank Leaching Procedure characterization leaching of inorganic compounds NA tank leaching monolithic and compacted granular solid materials July 2017
1316 Liquid-Solid Partitioning as a Function of Liquid-Solid Ratio Using a Parallel Batch Extraction Procedure characterization leaching of inorganic compounds NA batch extraction solid materials July 2017
1320 Multiple Extraction Procedure characterization leaching of waste caused by acid rain NA multiple extractions Liquids, solids, multiphase wastes Sept. 1986
1330A Extraction Procedure for Oily Wastes characterization mobile metals NA Soxhlet Extraction oily wastes: API separator sludges, rag oils, slop oil emulsions, other oil wastes from petroleum refining July 1992
1340 In Vitro Bioaccessibility Assay for Lead in Soil characterization lead (Pb) 7439-92-1 Extraction soil Feb. 2017
3005A Acid Digestion of Waters for Total Recoverable or Dissolved Metals for Analysis by FLAA or ICP Spectroscopy sample preparation heavy metals: aluminum (Al), antimony (Sb), arsenic (As), Barium (Ba), beryllium (Be), cadmium (Cd), calcium (Ca), chromium (Cr), cobalt (Co), copper (Cu), iron (Fe), lead (Pb), magnesium (Mg), manganese (Mn), molybdenum (Mo), nickel (Ni), potassium (K), selenium (Se), silver (Ag), sodium (Na), thallium (Tl), vanadium (V), zinc (Zn) Al: 7429-90-5, Sb: 7440-36-0, As: 7440-38-2, Ba: 7440-39-3, Be: 7440-41-7, Cd: 7440-43-9, Ca: 7440-70-2, Cr: 7440-47-3, Co: 7440-48-4, Cu: 7440-50-8, Fe: 7439-89-6, Pb: 7439-92-1, Mg: 7439-95-4, Mn: 7439-96-5, Mo: 7439-98-7, Ni: 7440-02-0, K: 7440-09-7, Se: 7782-49-2, Ag: 7440-22-4, Na: 7440-23-5, Tl: 7440-28-0, V: 7440-62-2, Zn: 7440-66-6 acid digestion surface water, ground water July 1992
3010A Acid Digestion of Aqueous Samples and Extracts for Total Metals for Analysis by FLAA or ICP Spectroscopy sample preparation heavy metals: aluminum (Al), antimony (Sb), arsenic (As), Barium (Ba), beryllium (Be), cadmium (Cd), calcium (Ca), chromium (Cr), cobalt (Co), copper (Cu), iron (Fe), lead (Pb), magnesium (Mg), manganese (Mn), molybdenum (Mo), nickel (Ni), potassium (K), selenium (Se), silver (Ag), sodium (Na), thallium (Tl), vanadium (V), zinc (Zn) Al: 7429-90-5, Sb: 7440-36-0, As: 7440-38-2, Ba: 7440-39-3, Be: 7440-41-7, Cd: 7440-43-9, Ca: 7440-70-2, Cr: 7440-47-3, Co: 7440-48-4, Cu: 7440-50-8, Fe: 7439-89-6, Pb: 7439-92-1, Mg: 7439-95-4, Mn: 7439-96-5, Mo: 7439-98-7, Ni: 7440-02-0, K: 7440-09-7, Se: 7782-49-2, Ag: 7440-22-4, Na: 7440-23-5, Tl: 7440-28-0, V: 7440-62-2, Zn: 7440-66-6 acid digestion aqueous samples, extracts, wastes with suspended solids July 1992
3015A Microwave Assisted Acid Digestion of Aqueous Samples and Extracts sample preparation heavy metals: aluminum (Al), antimony (Sb), arsenic (As), Barium (Ba), beryllium (Be), boron (B), cadmium (Cd), calcium (Ca), chromium (Cr), cobalt (Co), copper (Cu), iron (Fe), lead (Pb), magnesium (Mg), manganese (Mn), mercury (Hg), molybdenum (Mo), nickel (Ni), potassium (K), selenium (Se), silver (Ag), sodium (Na), strontium (Sr), thallium (Tl), vanadium (V), zinc (Zn) Al: 7429-90-5, Sb: 7440-36-0, As: 7440-38-2, Ba: 7440-39-3, Be: 7440-41-7, B: 7440-42-8, Cd: 7440-43-9, Ca: 7440-70-2, Cr: 7440-47-3, Co: 7440-48-4, Cu: 7440-50-8, Fe: 7439-89-6, Pb: 7439-92-1, Mg: 7439-95-4, Mn: 7439-96-5, Hg: 7439-97-6, Mo: 7439-98-7, Ni: 7440-02-0, K: 7440-09-7, Se: 7782-49-2, Ag: 7440-22-4, Na: 7440-23-5, Sr: 7440-24-6, Tl: 7440-28-0, V: 7440-62-2, Zn: 7440-66-6 Microwave Assisted Acid Digestion aqueous samples, drinking water, extracts, wastes with suspended solids Feb. 2007
3020A Acid Digestion of Aqueous Samples and Extracts for Total Metals for Analysis by GFAA Spectroscopy sample preparation heavy metals: beryllium (Be), cadmium (Cd), chromium (Cr), cobalt (Co), lead (Pb), molybdenum (Mo), thallium (Tl), vanadium (V) Be: 7440-41-7, Cd: 7440-43-9, Cr: 7440-47-3, Co: 7440-48-4, Pb: 7439-92-1, Mo: 7439-98-7, Tl: 7440-28-0, V: 7440-62-2, Zn: 7440-66-6 acid digestion aqueous samples, extracts, wastes with suspended solids July 1992
3031 Acid Digestion of Oils for Metals Analysis by Atomic Absorption or ICP Spectrometry sample preparation heavy metals: antimony (Sb), arsenic (As), Barium (Ba), beryllium (Be), cadmium (Cd), chromium (Cr), cobalt (Co), copper (Cu), lead (Pb), molybdenum (Mo), nickel (Ni), potassium (K), selenium (Se), silver (Ag), sodium (Na), strontium (Sr), thallium (Tl), vanadium (V), zinc (Zn) Sb: 7440-36-0, As: 7440-38-2, Ba: 7440-39-3, Be: 7440-41-7, Cd: 7440-43-9, Cr: 7440-47-3, Co: 7440-48-4, Cu: 7440-50-8, Pb: 7439-92-1, Mo: 7439-98-7, Ni: 7440-02-0, K: 7440-09-7, Se: 7782-49-2, Ag: 7440-22-4, Na: 7440-23-5, Sr: 7440-24-6, Tl: 7440-28-0, V: 7440-62-2, Zn: 7440-66-6 acid digestion oils, oil sludges, tars, waxes, paints, paint sludges, other viscous petroleum products Dec. 1996
3040A Dissolution Procedure for Oils, Greases, or Waxes sample preparation heavy metals: antimony (Sb), arsenic (As), Barium (Ba), beryllium (Be), cadmium (Cd), chromium (Cr), copper (Cu), iron (Fe), lead (Pb), manganese (Mn), nickel (Ni), vanadium (V) Sb: 7440-36-0, As: 7440-38-2, Ba: 7440-39-3, Be: 7440-41-7, Cd: 7440-43-9, Cr: 7440-47-3, Cu: 7440-50-8, Fe: 7439-89-6, Pb: 7439-92-1, Mn: 7439-96-5, Ni: 7440-02-0, V: 7440-62-2 solvent dissolution oils, greases, waxes Dec. 1996
3050B Acid Digestion of Sediments, Sludges, and Soils sample preparation heavy metals: aluminum (Al), antimony (Sb), arsenic (As), Barium (Ba), beryllium (Be), cadmium (Cd), calcium (Ca), chromium (Cr), cobalt (Co), copper (Cu), iron (Fe), lead (Pb), magnesium (Mg), manganese (Mn), molybdenum (Mo), nickel (Ni), potassium (K), selenium (Se), silver (Ag), sodium (Na), thallium (Tl), vanadium (V), zinc (Zn) Al: 7429-90-5, Sb: 7440-36-0, As: 7440-38-2, Ba: 7440-39-3, Be: 7440-41-7, Cd: 7440-43-9, Ca: 7440-70-2, Cr: 7440-47-3, Co: 7440-48-4, Cu: 7440-50-8, Fe: 7439-89-6, Pb: 7439-92-1, Mg: 7439-95-4, Mn: 7439-96-5, Mo: 7439-98-7, Ni: 7440-02-0, K: 7440-09-7, Se: 7782-49-2, Ag: 7440-22-4, Na: 7440-23-5, Tl: 7440-28-0, V: 7440-62-2, Zn: 7440-66-6 acid digestion Sediments, Sludges, and Soils Dec. 1996
3051A Microwave Assisted Acid Digestion of Sediments, Sludges, Soils, and Oils sample preparation heavy metals: aluminum (Al), antimony (Sb), arsenic (As), Barium (Ba), beryllium (Be), boron (B), cadmium (Cd), calcium (Ca), chromium (Cr), cobalt (Co), copper (Cu), iron (Fe) Al: 7429-90-5, Sb: 7440-36-0, As: 7440-38-2, Ba: 7440-39-3, Be: 7440-41-7,B: 7440-42-8, Cd: 7440-43-9, Ca: 7440-70-2, Cr: 7440-47-3, Co: 7440-48-4, Cu: 7440-50-8, Fe: 7439-89-6 Microwave Assisted Acid Digestion Sediments, Sludges, Soils, and Oils Feb. 2007
3052 Microwave Assisted Acid Digestion of Siliceous and Organically Based Matrices sample preparation heavy metals: aluminum (Al), antimony (Sb), arsenic (As), Barium (Ba), beryllium (Be), cadmium (Cd), calcium (Ca), chromium (Cr), cobalt (Co), copper (Cu), iron (Fe), lead (Pb), magnesium (Mg), manganese (Mn), molybdenum (Mo), nickel (Ni), potassium (K), selenium (Se), silver (Ag), sodium (Na), thallium (Tl), vanadium (V), zinc (Zn) Al: 7429-90-5, Sb: 7440-36-0, As: 7440-38-2, Ba: 7440-39-3, Be: 7440-41-7, Cd: 7440-43-9, Ca: 7440-70-2, Cr: 7440-47-3, Co: 7440-48-4, Cu: 7440-50-8, Fe: 7439-89-6, Pb: 7439-92-1, Mg: 7439-95-4, Mn: 7439-96-5, Mo: 7439-98-7, Ni: 7440-02-0, K: 7440-09-7, Se: 7782-49-2, Ag: 7440-22-4, Na: 7440-23-5, Tl: 7440-28-0, V: 7440-62-2, Zn: 7440-66-6 Microwave Assisted Acid Digestion siliceous matrices, organic matrices, and other complex matrices Dec. 1996
3060A Alkaline Digestion for Hexavalent Chromium sample preparation Hexavalent Chromium 18540-29-9 Alkaline Digestion solid waste, soils, sludges, sediment Dec. 1996
3200 Mercury Species Fractionation and Quantification by Microwave Assisted Extraction, Selective Solvent Extraction and/or Solid Phase Extraction sample preparation Mercury species: methylmercury chloride (CH3HgCl), ethylmercury chloride (CH3CH2HgCl), mercury(II) chloride (HgCl2), mercury hydroxide (Hg(OH)2), mercury nitrate (Hg(NO3)3), mercury sulfate (HgSO4), mercury oxide (HgO), Hg2+ complexes, elemental mercury (Hg0), mercury-metal almalgams (Hg0-M), mercury(I) chloride (Hg2Cl2), mercury sulfide (HgS), mercury selenide (HgSe) CH3HgCl: 115-09-3, CH3CH2HgCl: 107-27-7, HgCl2: 7487-94-7, Hg(NO3)2: 10045-94-0, HgSO4, 13766-44-4, HgO: 21908-53-2, Hg0: 7439-97-6, Hg2Cl2: 10112-91-1, HgS: 1344-48-5, HgSe: 20601-83-6 Microwave Assisted Extraction, Selective Solvent Extraction, Solid Phase Extraction soils, sediments July 2014
3500C Organic Extraction and Sample Preparation sample preparation guidance semivolatile organics, nonvolatile organics NA Extraction aqueous and solid samples Feb. 2007
3510C Separatory Funnel Liquid-Liquid Extraction sample preparation organic compounds NA Separatory Funnel Liquid-Liquid Extraction aqueous samples Dec. 1996
3511 Organic Compounds in Water by Microextraction sample preparation Volatile Organic Compounds (VOCs) and Semivolatile Organic Compounds (SVOCs) NA Microextracion water July 2014
3520C Continuous Liquid-Liquid Extraction sample preparation organic NA Continuous Liquid-Liquid Extraction aqueous samples Dec. 1996
3535A Solid-Phase Extraction (SPE) sample preparation organic groups: Phthalate esters, Organochlorine pesticides, Polychlorinated biphenyls (PCBs), Organophosphorus pesticides, Nitroaromatics and nitramines, Explosives, TCLP leachates containing organochlorine pesticides, TCLP leachates containing semivolatiles, TCLP leachates containing phenoxyacid herbicides NA solid-phase extraction (SPE) aqueous samples Feb. 2007
3540C Soxhlet Extraction sample preparation nonvolatile and semivolatile organic compounds NA Soxhlet extraction soils, sludges, solid wastes Dec. 1996
3541 Automated Soxhlet Extraction sample preparation organic analytes NA Automated Soxhlet Extraction soil, sediment, sludges, solid waste Sept. 1994
3542 Extraction of Semivolatile Analytes Collected Using Method 0010 (Modified Method 5 Sampling Train) sample preparation semivolatile organic compounds NA Separatory Funnel & Soxhlet Extraction air sampling train Dec. 1996
3545A Pressurized Fluid Extraction (PFE) sample preparation water soluble organic compounds: semivolatiles, organophosphorus pesticides, organochlorine pesticides, chlorinated herbicides, polychlorinated biphenyls (PCBs), polychlorinated dibenzo-p-dioxins and polychlorinated dibenzofurans (PCDDs/PCDFs), and diesel range organics (DRO) NA pressurized fluid extraction (PFE) soils, sediments, sludges, solid waste, Feb. 2007
3546 Microwave Extraction sample preparation water insoluble organic compounds: semivolatiles, organophosphorus pesticides, organochlorine pesticides, chlorinated herbicides, phenoxyacid herbicides, substituted phenols, polychlorinated biphenyls (PCBs), and polychlorinated dibenzo-p-dioxins and polychlorinated dibenzofurans (PCDDs/PCDFs) NA Microwave Extraction/Soxhlet extraction soils, clays, sediments, sludges, solid waste Feb. 2007
3550C Ultrasonic Extraction sample preparation nonvolatile and semivolatile organic compounds NA Ultrasonic Extraction soils, sludges, wastes Feb. 2007
3560 Supercritical Fluid Extraction of Total Recoverable Petroleum Hydrocarbons sample preparation total recoverable petroleum hydrocarbons (TRPHs) NA supercritical fluid extraction (SFE) soils, sediments, fly ash, solid-phase extraction media Dec. 1996
3561 Supercritical Fluid Extraction of Polynuclear Aromatic Hydrocarbons sample preparation polynuclear aromatic hydrocarbons (PAHs): acenaphthene, acenaphthylene, anthracene, benz(a)anthracene, benzo(b)fluoranthene, benzo(k)fluoranthene, benzo(g,h,i)perylene, benzo(a)pyrene, chrysene, dibenzo(a,h)anthracene, fluoranthene, fluorene, indeno(1,2,3-cd)pyrene, naphthalene, phenanthrene, pyrene 83-32-9, 208-96-8, 120-12-7, 56-55-3, 205-99-2, 207-08-9, 191-24-2, 50-32-8, 218-01-9, 53-70-3, 206-44-0, 86-73-7, 193-39-5, 91-20-3, 85-01-8, 129-00-0 supercritical fluid extraction (SFE) soils, sediments, fly ash, solid-phase extraction media Dec. 1996
3562 Supercritical Fluid Extraction of Polychlorinated Biphenyls (PCBs) and Organochlorine Pesticides sample preparation polychlorinated biphenyls (PCBs) and organochlorine pesticides (OCPs): 2,4,4'-Trichlorobiphenyl, 2,2',5,5'-Tetrachlorobiphenyl, 2,2',4,5,5'-Pentachlorobiphenyl , 2,3,3',4,4'-Pentachlorobiphenyl, 2,3',4,4',5-Pentachlorobiphenyl, 2,2',3,3',4,4'-Hexachlorobiphenyl, 2,2',3,4,4',5'-Hexachlorobiphenyl, 2,2',3,4',5',6-Hexachlorobiphenyl, 2,2',4,4',5,5'-Hexachlorobiphenyl, 2,3,3',4,4',5'-Hexachlorobiphenyl, 2,2',3,3',4,4',5-Heptachlorobiphenyl, 2,2',3,4,4',5,5'-Heptachlorobiphenyl, Aldrin, ?-Hexachlorocyclohexane (?-BHC), ?-Hexachlorocyclohexane (?-BHC), ?-Hexachlorocyclohexane (?-BHC, or Lindane), ?-Chlordane, 4,4'-DDD, 4,4'-DDE, 4,4'-DDT, Dieldrin, Endosulfan II, Endrin, Endrin aldehyde, Heptachlor, Heptachlor epoxide 7012-37-5, 35693-99-3, 37680-73-2, 32598-14-4, 31508-00-6, 38380-07-3, 35065-28-2, 38380-04-0, 35065-27-1, 38380-08-4, 35065-30-6, 35065-29-3, 309-00-2, 319-85-7, 319-86-8, 58-89-9, 5103-71-9, 72-54-8, 72-55-9, 50-29-3, 60-57-1, 33213-65-9, 72-20-8, 7421-93-4, 76-44-8, 1024-57-3 supercritical fluid extraction (SFE) soils, sediments, fly ash, solid-phase extraction media Feb. 2007
3572 Extraction of Chemical Agents from Wipe Samples Using Microextraction sample preparation GB (o-Isopropyl methylphosphonofluoridate), VX (O-Ethyl S-2-diisopropylaminoethyl methyl phosphonothiolate), HD [Bis(2-chloroethyl)sulfide] GB: 107-44-8, VX: 50782-69-9, HD: 505-60-2 Microextracion wipe samples July 2014
3580A Waste Dilution sample preparation organic compounds with concentration > 20,000 mg/kg NA solvent dilution non-aqueous wastes July 1992
3585 Waste Dilution for Volatile Organics sample preparation volatile organic compounds (VOCs) with concentration > 1 mg/kg NA solvent dilution non-aqueous wastes Dec. 1996
3600C Cleanup sample cleanup guidance NA NA cleanup sample extracts Dec. 1996
3610B Alumina Cleanup sample cleanup phthalate esters, nitrosamines NA separation (alumina) sample extracts Dec. 1996
3611B Alumina Column Cleanup and Separation of Petroleum Wastes sample cleanup organic analytes NA chromatographic separation (alumina) sample extracts Dec. 1996
3620C Florisil Cleanup sample cleanup phthalate esters, nitrosamines, nitroaromatics, haloethers, aniline & derivatives, chlorinated hydrocarbons, organochlorine pesticides, organophosphates, organophosphorus pesticides, polychlorinated biphenyls (PCBs) NA separation (Florisil®) sample extracts July 2014
3630C Silica Gel Cleanup sample cleanup polynuclear aromatic hydrocarbons (PAHs), derivatized phenolic compounds, organochlorine pesticides, polychlorinated biphenyls (PCBs) as Aroclors, pentafluorobenzyl bromide-derivatized phenols NA separation (silica gel) sample extracts Dec. 1996
3640A Gel-Permeation Cleanup sample cleanup acenaphthene, acenaphthlylene, acetophenone, 2-acetylaminofluorene, aldrin, 4-aminobiphenyl, aniline, anthracene, benomyl, benzenethiol, benzidine, benz(a)anthracene, benzo(b)fluoranthene, benzo(a)pyrene, benzo(k)fluoranthene, benzoic acid, benzotrichloride, benzyl alcohol, benzyl chloride, alpha-BHC, beta-BHC, gamma-BHC, delta-BHC, 4-bromophenyl phenyl ether, butyl benzyl phthalate, 2-sec-butyl-4,6-dinitrophenol (Dinoseb), carbazole, carbendazim, alpha-chlordane, gamma-chlordane, 4-chloro-3-methylphenol, 4-chloroaniline, chlorobenzilate, bis(2-chloroethoxy)methane, bis(2-chloroethyl)ether, bis(2-chloroisopropyl)ether, 2-chloronaphthalene, 2-chlorophenol, 4-chlorophenol, 3-chlorophenol, 4-chlorophenyl phenyl ether, 3-chloropropionitrile, chrysene, 2-cresol, 3-cresol, 4-cresol, cyclophosphamide, DDD, DDE, DDT, di-n-butyl phthalate, diallate, dibenzo(a,e)pyrene, dibenzo(a,i)pyrene, dibenzo(a,j)acridine, dibenzo(a,h)anthracene, dibenzofuran, dibenzothiophene, 1,2-dibromo-3-chloropropane, 1,2-dibromoethane, trans-1,4-dichloro-2-butene, cis-1,4-dichloro-2-butene, 1,2-dichlorobenzene, 1,3-dichlorobenzene, 1,4-dichlorobenzene, 3,3'-dichlorobenzidine, 2,6-dichlorophenol, 2,4-dichlorophenoxyacetic acid (2,4-D), 2,4-dichlorophenol, 2,4-dichlorotoluene, 1,3-dichloro-2-propanol, dieldrin, diethyl phthalate, dimethoate, dimethyl phthalate, p-dimethylaminoazobenzene, 7,12-dimethyl-benz(a)anthracene, 2,4-dimethylphenol, 3,3-dimethylbenzidine, 4,6-dinitrobenzene, 4,6-dinitro-o-cresol, 1,3-dinitrobenzene, 2,4-dinitrophenol, 2,4-dinitrotoluene, 2,6-dinitrotoluene, diphenylamine, diphenyl ether, 1,2-diphenylhydrazine, disulfoton, endosulfan sulfate, endosulfan I, endosulfan II, endrin, endrin aldehyde, endrin ketone, ethyl methane sulfonate, ethyl methacrylate, bis(2-ethylhexyl)phthalate, famphur, fluorene, fluoranthene, heptachlor, heptachlor epoxide, hexachlorobenzene, hexachlorobutadiene, hexachlorocyclopentadiene, hexachloroethane, hexachloropropene, indeno(1,2,3-cd)pyrene, isodrin, isophorone, cis-isosafrole, trans-isosafrole, kepone, malononitrile, merphos, methoxychlor, 3-methylcholanthrene, 2-methylnaphthalene, methyl parathion, 4,4'-methylene-bis(2-chloroaniline), naphthalene, 1,4-naphthoquinone, 2-naphthylamine, 1-naphthylamine, 5-nitro-o-toluidine, 2-nitroaniline, 3-nitroaniline, 4-nitroaniline, nitrobenzene, 2-nitrophenol, 4-nitrophenol, n-nitrosodi-n-butylamine, n-nitrosodiethanolamine, n-nitrosodiethylamine, n-nitrosodimethylamine, n-nitrosodiphenylamine, n-nitrosodi-n-propylamine, n-nitrosomethylethylamine, n-nitrosomorpholine, n-nitrosopiperidine, n-nitrosopyrolidine, di-n-octyl phthalate, parathion, pentachlorobenzene, pentachloroethane, pentachloronitrobenzene (PCNB), pentachlorophenol, phenacetin, phenanthrene, phenol, 1,2-phenylenediamine, phorate, 2-picoline, pronamide, pyrene, resorcinol, safrole, 1,2,4,5-tetrachlorobenzene, 2,3,5,6-tetrachloronitrobenzene, 2,3,5,6-tetrachlorophenol, 2,3,4,6-tetrachlorophenol, tetratheyl dithiopyrophosphate (Sulfotep), thiosemicarbazide, 2-toluidine, 4-toluidine, thiourea,1-(o-chlorophenyl), toluene-2,4-diamine, 1,2,3-trichlorobenzene, 1,2,4-trichlorobenzene, 2,4,6-trichlorophenol, 2,4,5-trichlorophenol, 2,4,5-trichlorophenoxyacetic acid (2,4,5-T), 2,4,5-trichlorophenoxypropionic acid (2,4,5-TP), warfarin 83-32-9, 208-96-8, 98-86-2, 53-96-3, 309-00-2, 92-67-1, 62-53-3, 120-12-7, 17804-35-2, 108-98-5, 92-87-5, 56-55-3, 205-99-2, 50-32-8, 191-24-2, 207-08-9, 65-85-0, 98-07-7, 100-51-6, 100-44-7, 319-84-6, 319-85-7, 58-89-9, 319-86-8, 101-55-3, 85-68-7, 88-85-7, 86-74-8, 10605-21-7, 5103-71-9, 5566-34-7, 59-50-7, 106-47-8, 510-15-6, 111-91-1, 111-44-4, 108-60-1, 91-58-7, 95-57-8, 106-48-9, 108-43-0, 7005-72-3, 542-76-7, 218-01-9, 95-48-7, 108-39-4, 106-44-5, 50-18-0, 72-54-8, 72-55-9, 50-29-3, 84-74-2, 2303-16-4, 192-65-4, 189-55-9, 224-42-0, 53-70-3, 132-64-9, 132-65-0, 96-12-8, 106-93-4, 110-57-6, 1476-11-5, 95-50-1, 106-46-7, 541-73-1, 91-94-1, 87-65-0, 94-75-7, 120-83-2, 95-73-8, 96-23-1, 60-57-1, 84-66-2, 60-51-5, 131-11-3, 60-11-7, 57-97-6, 105-67-9, 119-93-7, 534-52-1, 99-65-0, 51-28-5, 121-14-2, 606-20-2, 122-39-4, 101-84-8, 122-66-7, 298-04-4, 1031-07-8, 959-98-8, 33213-65-9, 72-20-8, 7421-93-4, 53494-70-5, 62-50-0, 97-63-2, 117-81-7, 52-85-7, 86-73-7, 206-44-0, 76-44-8, 1024-57-3, 118-74-1, 87-68-3, 77-47-4, 67-72-1, 1888-71-7, 193-39-5, 465-73-6, 78-59-1, 17627-76-8, 4043-71-4, 143-50-0, 109-77-3, 150-50-5, 72-43-5, 56-49-5, 91-57-6, 298-00-0, 101-14-4, 91-20-3, 130-15-4, 91-59-8, 134-32-7, 99-55-8, 88-74-4, 99-09-2, 100-01-6, 98-95-3, 79-46-9, 100-02-7, 924-16-3, 1116-54-7, 55-18-5, 62-75-9, 86-30-6, 621-64-7, 10595-95-6, 59-89-2, 100-75-4, 930-55-2, 117-84-0, 56-38-2, 608-93-5, 76-01-7, 82-68-8, 87-86-5, 62-44-2, 85-01-8, 108-95-2, 95-54-5, 298-02-2, 109-06-8, 23950-58-5, 129-00-0, 108-46-3, 94-59-7, 95-94-3, 117-18-0, 935-95-5, 58-90-2, 3689-24-5, 79-19-6, 106-49-0, 95-53-4, 5344-82-1, 95-80-7, 87-61-6, 120-82-1, 88-06-2, 95-95-4, 93-76-5, 93-72-1, 81-81-2 gel-permeation chromatography (GPC) sample extracts Sept. 1994
3650B Acid-Base Partition Cleanup sample cleanup benz(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene, chlordane, chlorinated dibenzodioxins, 2-chlorophenol, chrysene, creosote, cresols, dichlorobenzenes, dichlorophenoxyacetic acid, 2,4-dimethylphenol, dinitrobenzene, 4,6-dinitro-o-cresol, 2,4-dinitrotoluene, heptachlor, hexachlorobenzene, hexachlorobutadiene, hexachloroethane, hexachlorocyclopentadiene, naphthalene, nitrobenzene, 4-nitrophenol, pentachlorophenol, phenol, phorate, 2-picoline, pyridine, tetrachlorobenzenes, tetrachlorophenols, toxaphene, trichlorophenols, 2,4,5-TP (Silvex) 56-55-3, 50-32-8, 205-99-2, 57-74-9, 95-57-8, 218-01-9, 8001-58-9, 94-75-7, 105-67-9, 25154-54-5, 534-52-1, 121-14-2, 76-44-8, 118-74-1, 87-68-3, 67-72-1, 77-47-4, 91-20-3, 98-95-3, 100-02-7, 87-86-5, 108-95-2, 298-02-2, 109-06-8, 110-86-1, 8001-35-2, 93-72-1, and others liquid-liquid partitioning petroleum waste, sample extracts Dec. 1996
3660B Sulfur Cleanup sample cleanup organochlorine pesticides, organophosphorus pesticides NA sulfur removal sediments, marine algae, and industrial wastes containing sulfur Dec. 1996
3665A Sulfuric Acid/Permanganate Cleanup sample cleanup polychlorinated biphenyls (PCBs) NA separation (sulfuring acid) sample extracts Dec. 1996
3815 Screening Solid Samples for Volatile Organics screening volatile organic compounds (VOCs) NA photoionization detection (PID) soils, solids Feb. 2007
3820 Hexadecane Extraction and Screening of Purgeable Organics screening purgeable organics NA hexadecane extraction and gas chromatography/ flame-ionization detection (GC/FID) not specified Sept. 1986
4000 Immunoassay screening guidance organic and inorganic analytes NA Immunoassay environmental and waste matrices Dec. 1996
4010A Screening for Pentachlorophenol by Immunoassay screening pentachlorophenol (PCP) 87-86-5 Immunoassay soils, sludges, aqueous media Dec. 1996
4015 Screening for 2,4-Dichlorophenoxyacetic Acid by Immunoassay screening 2,4-dichloropyhenoxyacetic acid (2,4-D) 94-75-7 Immunoassay soils, aqueous matrices Dec. 1996
4020 Screening for Polychlorinated Biphenyls by Immunoassay screening polychlorinated biphenyls (PCBs) NA Immunoassay soils, non-aqueous liquid waste Dec. 1996
4025 Screening for Polychlorinated Dibenzodioxins and Polychlorinated Dibenzofurans (PCDD/PCDFs) By Immunoassay screening Polychlorinated Dibenzodioxins (PCDDs) and Polychlorinated Dibenzofurans (PCDFs) NA Immunoassay soil July 2014
4030 Soil Screening for Petroleum Hydrocarbons by Immunoassay screening total petroleum hydrocarbons (TPH) NA Immunoassay soils Dec. 1996
4035 Soil Screening for Polynuclear Aromatic Hydrocarbons by Immunoassay screening polynuclear aromatic hydrocarbons (PAHs) NA Immunoassay soils Dec. 1996
4040 Soil Screening for Toxaphene by Immunoassay screening toxaphene 8001-35-2 Immunoassay soils Dec. 1996
4041 Soil Screening for Chlordane by Immunoassay screening Chlordane 57-74-9 Immunoassay soils Dec. 1996
4042 Soil Screening for DDT by Immunoassay screening 1,1,1-trichloro-2,2-bis(4-chlorophenyl)ethane (DDT) 50-29-3 Immunoassay soils Dec. 1996
4050 TNT Explosives in Soil by Immunoassay screening trinitrotoluene (TNT) 118-96-7 Immunoassay soils Dec. 1996
4051 Hexahydro-1,3,5-trinitro-1,3,5-triazine (RDX) in Soil by Immunoassay screening hexahydro-1,3,5-trinitro-1,3,5-triazine (RDX) 121-82-4 Immunoassay soils Dec. 1996
4425 Screening Extracts of Environmental Samples for Planar Organic Compounds (PAHs, PCBs, PCDDs/PCDFs) by a Reporter Gene on a Human Cell Line screening polychlorinated dibenzo-p-dioxins (PCDDs), polychlorinated dibenzofurans (PCDFs), coplanar polychlorinated biphenyl (PCB) congeners, high molecular weight polynuclear aromatic hydrocarbons (PAHs) NA reporter gene system (RGS) soil, sediment, tissue, and water extracts Feb. 2007
4430 Screening for Polychlorinated Dibenzo-p-dioxins and Poly chlorinated Dibenzofurans (PCDD/PCDFs) in Soil and Sediments Using an Aryl Hydrocarbon Receptor-Based PCR Assay screening Polychlorinated Dibenzodioxins (PCDDs) and Polychlorinated Dibenzofurans (PCDFs) NA Aryl Hydrocarbon Receptor-Based PCR Assay soil and sediments July 2014
4435 Screening for Dioxin-like Chemical Activity in Soils and Sediments Using the CALUX® Bioassay and TEQ Determinations screening Dioxin-like Chemicals NA CALUX® Bioassay and Toxic Equivalent (TEQ) Determinations soil and sediments July 2014
4670 Triazine Herbicides as Atrazine in Water by Quantitative Immunoassay determinative Atrazine 1912-24-9 Immunoassay water Feb. 2007
5000 Sample Preparation for Volatile Organic Compounds sample preparation guidance volatile organic compounds (VOCs) NA NA aqueous waste, soil, sediment, solid waste, organic solvents, air, oily waste Dec. 1996
5021A Volatile Organic Compounds in Various Sample Matrices Using Equilibrium Headspace Analysis sample preparation volatile organic compounds (VOCs): Benzene, Bromochloromethane, Bromodichloromethane, Bromoform, Bromomethane, Carbon tetrachloride, Chlorobenzene, Chloroethane, Chloroform, Chloromethane, Dibromochloromethane, 1,2-Dibromo-3-chloropropane, 1,2-Dibromoethane, Dibromomethane, 1,2-Dichlorobenzene, 1,3-Dichlorobenzene, 1,4-Dichlorobenzene, Dichlorodifluoromethane, 1,1-Dichloroethane, 1,2-Dichloroethane, 1,1-Dichloroethene, trans-1,2-Dichloroethene, 1,2-Dichloropropane, Ethylbenzene, Hexachlorobutadiene, Methylene chloride, Naphthalene, Styrene, 1,1,1,2-Tetrachloroethane, 1,1,2,2-Tetrachloroethane, Tetrachloroethene, Toluene, 1,2,4-Trichlorobenzene, 1,1,1-Trichloroethane, 1,1,2-Trichloroethane, Trichloroethene, Trichlorofluoromethane, 1,2,3-Trichloropropane, Vinyl chloride, o-Xylene, m-Xylene, p-Xylene, gasoline range organics, bromobenzene, n-butylbenzene, sec-butylbenzene, tert-butylbenzene, 2-chlorotoluene, 4-chlorotoluene, cis-1,2-dichloroethene, 1,3-dichloropropane, 2,2-dichloropropane, 1,1-dichloropropene, isopropylbenzene, 4-isoproyltoluene, n-propylbenzene, 1,2,3-trichlorobenzene, 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene 71-43-2, 74-97-5,75-27-4, 75-25-2, 74-83-9, 56-23-5,108-90-7, 75-00-3, 67-66-3, 74-87-3, 124-48-1,96-12-8, 106-93-4, 74-95-3, 95-50-1, 541-73-1, 106-46-7, 75-71-8, 75-34-3, 107-06-2, 75-35-4, 156-60-5, 78-87-5, 100-41-4, 87-68-3, 75-09-2, 91-20-3, 100-42-5, 630-20-6, 79-34-5, 127-18-4, 108-88-3, 120-82-1, 71-55-6, 79-00-5, 79-01-6, 75-69-4, 96-18-4, 75-01-4, 95-47-6, 108-38-3, 106-42-3, 108-86-1, 104-51-8, 135-98-8, 98-06-6, 95-49-8, 106-43-4, 156-59-4, 142-28-9, 590-20-7, 563-58-6, 98-82-8, 99-87-6, 103-65-1, 87-61-6, 95-63-6, 108-67-8 equilibrium headspace analysis soils, sediments, solid waste, aqueous samples, water-miscible liquids July 2014
5030B Purge-and-Trap for Aqueous Samples sample preparation volatile organic compounds (VOCs) with boiling points < 200 C NA purge-and-trap aqueous samples, water miscible liquid samples, soil and waste sample extracts Dec. 1996
5031 Volatile, Nonpurgeable, Water-Soluble Compounds by Azeotropic Distillation sample preparation nonpurgeable, water-soluble, and volatile organic compounds: Acetone, Acetonitrile, Acrylonitrile, Allyl alcohol, 1-Butanol, t-Butyl alcohol, Crotonaldehyde, 1,4-Dioxane, Ethanol, Ethyl Acetate, Ethylene oxide, Isobutyl alcohol, Methanol, Methyl ethyl ketone, Methyl isobutyl ketone, N-Nitroso-di-n-butylamine, Paraldehyde, 2-Pentanone, 2-Picoline, 1-Propanol, 2-Propanol, Propionitrile, Pyridine, o-Toluidine 67-64-1, 75-05-8, 107-13-1, 107-18-6, 104-51-8, 75-65-0, 123-73-9, 123-91-1, 64-17-5, 141-78-6, 75-21-8, 78-83-1, 67-56-1, 78-93-3, 108-10-1, 924-16-3, 123-63-7, 107-87-9, 109-06-8, 71-23-8, 67-63-0, 107-12-0, 110-86-1, 95-53-4 Azeotropic Distillation aqueous samples, leachates from solid matrices Dec. 1996
5032 Volatile Organic Compounds by Vacuum Distillation determinative volatile organic compounds (VOCs): Acetone, Acrolein, Acrylonitrile, Benzene, Bromodichloromethane, Bromoform, Bromomethane, 2-Butanone, Carbon disulfide, Carbon tetrachloride, Chlorobenzene, Chlorodibromomethane, Chloroethane, 2-Chloroethyl vinyl ether, Chloroform, Chloromethane, Dibromomethane, 1,4-Dichloro-2-butene, Dichlorodifluoromethane, 1,1-Dichloroethane, 1,2-Dichloroethane, 1,1-Dichloroethene, trans-1,2-Dichloroethene, 1,2-Dichloropropane, cis-1,3-Dichloropropene, trans-1,3-Dichloropropene, Ethanol, Ethylbenzene, Ethyl methacrylate, 2-Hexanone, Iodomethane, Methylene chloride, 4-Methyl-2-pentanone, Styrene, 1,1,2,2-Tetrachloroethane, Tetrachloroethene, Toluene, 1,1,1-Trichloroethane, 1,1,2-Trichloroethane, Trichloroethene, Trichlorofluoromethane, 1,2,3-Trichloropropane, Vinyl acetate, Vinyl chloride, m-Xylene, p-Xylene, o-Xylene 67-64-1, 107-02-8, 107-13-1, 71-43-2, 75-27-4, 75-25-2,74-83-9, 78-93-3, 75-15-0, 56-23-5, 108-90-7, 124-48-1,75-00-3, 110-75-8,67-66-3, 74-87-3, 74-95-3, 764-41-0, 75-71-8, 75-35-4, 107-06-2, 75-35-3, 156-60-5, 78-87-5, 10061-01-5, 10061-02-6, 64-17-5, 100-41-4, 97-63-2, 591-78-6, 74-88-4, 75-09-2, 108-10-1, 100-42-5, 79-34-5, 75-71-8, 75-35-4, 107-06-2, 75-35-3,156-60-5, 78-87-5, 10061-01-5, 10061-02-6,l 64-17-5, 100-41-4, 97-63-2, 591-78-6, 74-88-4, 75-09-2, 108-10-1, 100-42-5, 79-34-5 Vacuum Distillation liquids, solids, oily waste, animal tissues Dec. 1996
5035 Closed-System Purge-and-Trap and Extraction for Volatile Organics in Soil and Waste Samples sample preparation volatile organic compounds (VOCs) NA purge-and-trap, extraction soils, sediments, solid waste Dec. 1996
5041A Analysis for Desorption of Sorbent Cartridges from Volatile Organic Sampling Train (VOST) determinative non-polar organic compounds: Acetone, Acrylonitrile, Benzene, Bromodichloromethane, Bromoform, Bromomethane, Carbon disulfide, Carbon tetrachloride, Chlorobenzene, Chlorodibromomethane, Chloroethane, Chloroform, Chloromethane, Dibromomethane, 1,1-Dichloroethane, 1,2-Dichloroethane, 1,1-Dichloroethene, trans-1,2-Dichloroethene, 1,2-Dichloropropane, cis-1,3-Dichloropropene, trans-1,3-Dichloropropene, Ethylbenzene, Iodomethane, Methylene chloride, Styrene, 1,1,2,2-Tetrachloroethane, Tetrachloroethene, Toluene, 1,1,1-Trichloroethane, 1,1,2-Trichloroethane, Trichloroethene, Trichlorofluoromethane, 1,2,3-Trichloropropane, Vinyl chloride, Xylenes 67-64-1, 107-13-1, 71-43-2, 75-27-4, 75-25-2, 74-83-9, 75-15-0, 56-23-5, 108-90-7, 124-48-1, 75-00-3, 67-66-3, 74-87-3, 74-95-3, 75-35-3, 107-06-2, 75-35-4, 156-60-5, 78-87-5, 10061-01-5, 10061-02-6, 100-41-4, 74-88-4, 75-09-2, 100-42-5, 79-34-5, 127-18-4, 108-88-3, 71-55-6, 79-00-5 desorption sorbent cartridges from stack gas effluents Dec. 1996
5050 Bomb Preparation Method for Solid Waste sample preparation chlorine (Cl2) 7782-50-5 bomb oxidation solid waste, oily waste, fuels Sept. 1994
6010D Inductively Coupled Plasma-Optical Emissions Spectrometry determinative heavy metals: aluminum (Al), antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), boron (B) cadmium (Cd), calcium (Ca), chromium (Cr), cobalt (Co), copper (Cu), iron (Fe), lead (Pb), lithium (Li), magnesium (Mg). magnese (Mn), mercury (Hg), molybdenum (Mo), nickel (Ni), phosphorous (P), potassium (K), selenium (Se), silica (SiO2), silver (Ag), sodium (Na), strotium (Sr), thallium (Tl), tin (Sn), titanium (Ti), vanadium (V), zinc (Zn) Al: 7429-90-5, Sb: 7440-36-0, As: 7440-38-2, Ba: 7440-39-3, Be: 7440-41-7, Cd: 7440-43-9, Ca: 7440-70-2, Cr: 7440-47-3, Co: 7440-48-4, Cu: 7440-50-8, Fe: 7439-89-6, Pb: 7439-92-1, Li: 7439-93-2, Mg: 7439-95-4, Mn: 7439-96-5, Hg: 7439-97-6, Mo: 7439-98-7, Ni: 7440-02-0, P: 7723-14-0, K: 7440-09-7, Se: 7782-49-2, SiO2: 7631-86-9, Ag: 7440-22-4, Na: 7440-23-5, Sr: 7440-24-6, Tl: 7440-28-0, Sn: 7440-31-5, Ti: 7440-32-6V: 7440-62-2, Zn: 7440-66-6 Inductively Coupled Plasma-Atomic (or Optical) Emission Spectrometry (ICP-AES or ICP-OES) groundwater, digested aqueous and solid matrices July 2018
6020B Inductively Coupled Plasma-Mass Spectrometry determinative heavy metals: aluminum (Al), antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), cadmium (Cd), calcium (Ca), chromium (Cr), cobalt (Co), copper (Cu), iron (Fe), lead (Pb), magnesium (Mg), manganese (Mn), mercury (Hg), nickel (Ni), potassium (K), selenium (Se), silver (Ag), sodium (Na), thallium (Tl), vanadium (V), zinc (Zn) Al: 7429-90-5, Sb: 7440-36-0, As: 7440-38-2, Ba: 7440-39-3, Be: 7440-41-7, Cd: 7440-43-9, Ca: 7440-70-2, Cr: 7440-47-3, Co: 7440-48-4, Cu: 7440-50-8, Fe: 7439-89-6, Pb: 7439-92-1,Mg: 7439-95-4, Mn: 7439-96-5, Hg: 7439-97-6, Ni: 7440-02-0, K: 7440-09-7, Se: 7782-49-2, Ag: 7440-22-4, Na: 7440-23-5, Tl: 7440-28-0, V: 7440-62-2, Zn: 7440-66-6 Inductively coupled plasma-mass spectrometry (ICP-MS) water samples, waste extracts, digests July 2014
6200 Field Portable X-Ray Fluorescence Spectrometry for the Determination of Elemental Concentrations in Soil and Sediment Determinative heavy metals: antimony (Sb), arsenic (As), barium (Ba), cadmium (Cd), calcium (Ca), chromium (Cr), cobalt (Co), copper (Cu), lead (Pb), mercury (Hg), nickel (Ni), selenium (Se), silver (Ag), thallium (Tl), tin (Sn), vanadium (V), zinc (Zn), iron (Fe), manganese (Mn), molybdenum (Mo), potassium (K), rubidium (Rb), strontium (Sr), thorium (Th), titanium (Ti), zirconium (Zr) Sb: 7440-36-0, As: 7440-38-2, Ba: 7440-39-3, Cd: 7440-43-9, Ca: 7440-70-2, Cr: 7440-47-3, Co: 7440-48-4, Cu: 7440-50-8, Pb: 7439-92-1, Hg: 7439-97-6, Ni: 7440-02-0, Se: 7782-49-2, Ag: 7440-22-4, Tl: 7440-28-0, Sn: 7440-31-5, V: 7440-62-2, Zn: 7440-66-6, 7439-89-6, 7439-96-5, 7439-93-7, 7440-09-7, 7440-17-7, 7440-24-6, 7440-29-1, 7440-32-6, 7440-67-7 X-ray Fluorescence soils, sediment Feb. 2007
6500 Dissolved Inorganic Anions in Aqueous Matrices by Capillary Ion Electrophoresis Determinative inorganic anions: bromide, chloride, fluoride, nitrate, nitrite, o-phosphate, sulfate 24959-67-9, 16887-00-6, 16984-48-8, 14797-55-8, 14797-65-0, 14265-44-2, 14808-79-8 Capillary Ion Electrophoresis aqueous matrices: drinking water, wastewater, ground water) Feb. 2007
6800 Elemental and Molecular Speciated Isotope Dilution Mass Spectrometry determinative heavy metals: antimony (Sb), boron (B), barium (Ba), cadmium (Cd), calcium (Ca), chromium (Cr), copper (Cu), iron (Fe), lead (Pb), magnesium (Mg), mercury (Hg), molybdenum (Mo), nickel (Ni), potassium (K), selenium (Se), silver (Ag), strontium (Sr), thallium (Tl), vanadium (V), zinc (Zn) Sb: 7440-36-0, B: 7440-42-8, Ba: 7440-39-3, Cd: 7440-43-9, Ca: 7440-70-2, Cr: 7440-47-3, Cu: 7440-50-8, Fe: 7439-89-6, Pb: 7439-92-1, Mg: 7439-95-4, Hg: 7439-97-6, Ni: 7440-02-0, K: 7440-09-7, Se: 7782-49-2, Ag: 7440-22-4, Sr: 7440-24-6, Tl: 7440-28-0, V: 7440-62-2, Zn: 7440-66-6 isotope dilution mass spectrometry (IDMS), molecular speciated isotope dilution mass spectrometry (SIDMS) water samples, solid samples, extracts, digests, blood, foods July 2014
7000B Flame Atomic Absorption Spectrophotometry Determinative heavy metals: aluminum (Al), antimony (Sb), Barium (Ba), beryllium (Be) cadmium (Cd), calcium (Ca), chromium (Cr), cobalt (Co), copper (Cu), iron (Fe), lead (Pb), lithium (Li), magnesium (Mg), manganese (Mn), mercury (Hg), molybdenum (Mo), nickel (Ni), osmium (Os), potassium (K), silver (Ag), sodium (Na), strontium (Sr), thallium (Tl), tin (Sn), vanadium (V), zinc (Zn) Al: 7429-90-5, Sb: 7440-36-0, Ba: 7440-39-3, Be: 7440-41-7, Cd: 7440-43-9, Ca: 7440-70-2, Cr: 7440-47-3, Co: 7440-48-4, Cu: 7440-50-8, Fe: 7439-89-6, Pb: 7439-92-1, Li: 7439-93-2, Mg: 7439-95-4, Mn: 7439-96-5, Hg: 7439-97-6, Mo: 7439-98-7, Ni: 7440-02-0, Os: 7440-04-2, K: 7440-09-7, Ag: 7440-22-4, Na: 7440-23-5, Sr: 7440-24-6, Tl: 7440-28-0, Sn: 7440-31-5, V: 7440-62-2, Zn: 7440-66-6 flame atomic absorption spectrophotometry (FLAA or FAAS) groundwater, aqueous samples, extracts, industrial waste, soils, sludges, sediments Feb. 2007
7010 Graphite Furnace Atomic Absorption Spectrophotometry Determinative heavy metals: , antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), cadmium (Cd), chromium (Cr), cobalt (Co), copper (Cu), iron (Fe), lead (Pb), manganese (Mn), molybdenum (Mo), nickel (Ni), selenium (Se), silver (Ag), thallium (Tl), vanadium (V), zinc (Zn) Sb: 7440-36-0, As: 7440-38-2, Ba: 7440-39-3, Be: 7440-41-7, Cd: 7440-43-9, Cr: 7440-47-3, Co: 7440-48-4, Cu: 7440-50-8, Fe: 7439-89-6, Pb: 7439-92-1, Mn: 7439-96-5, Mo: 7439-98-7, Ni: 7440-02-0, Se: 7782-49-2, Ag: 7440-22-4, Tl: 7440-28-0, Sn: 7440-31-5, V: 7440-62-2, Zn: 7440-66-6 graphite furnace atomic absorption spectrophotometry (GFAA or GFAAS) ground water, domestic wastes, industrial wastes, extracts, soils, sludges, sediments Feb. 2007
7061A Arsenic (Atomic Absorption, Gaseous Hydride) Determinative arsenic (As) 7440-38-2 Atomic Absorption Spectrophotometry (AAS) wastes, mobility procedure extracts, soils, ground water July 1992
7062 Antimony and Arsenic (Atomic Absorption, Borohydride Reduction) Determinative arsenic (As), antimony (Sb) 7440-38-2, 7440-36-0 Atomic Absorption Spectrophotometry (AAS) wastes, mobility procedure extracts, soils, ground water Sept. 1994
7063 Arsenic in Aqueous Samples and Extracts by Anodic Stripping Voltammetry (ASV) Determinative arsenic (As) 7440-38-2 anodic stripping voltammetry (ASV) drinking water, natural surface water, seawater, domestic/industrial wastewater, soil extracts Dec. 1996
7195 Chromium, Hexavalent (Coprecipitation) Determinative Hexavalent Chromium (Cr(VI)) 18540-29-9 Coprecipitation and atomic absorption spectroscopy (AAS) Extraction Procedure (EP) toxicity characteristic extracts, ground water Sept. 1986
7196A Chromium, Hexavalent (Chelation/Extraction) Determinative Hexavalent Chromium (Cr(VI)) 18540-29-9 colorimetry Extraction Procedure (EP) toxicity characteristic extracts, ground water July 1992
7197 Chromium, Hexavalent (Chelation/Extraction) Determinative Hexavalent Chromium (Cr(VI)) 18540-29-9 Chelation/Extraction and atomic absorption spectroscopy (AAS) Extraction Procedure (EP) toxicity characteristic extracts, ground water Sept. 1986
7198 Chromium, Hexavalent (Differential Pulse Polarography) Determinative Hexavalent Chromium (Cr(VI)) 18540-29-9 Differential Pulse Polarography natural waters, waste waters, extraction procedure (EP) extracts Sept. 1986
7199 Determination of Hexavalent Chromium in Drinking Water, Groundwater and Industrial Wastewater Effluents by Ion Chromatography Determinative Hexavalent Chromium (Cr(VI)) 18540-29-9 ion chromotography ground water, drinking water, industrial wastewater effluents Dec. 1996
7470A Mercury in Liquid Waste (Manual Cold-Vapor Technique) Determinative Mercury (Hg) 7439-97-6 Cold- vapor Atomic Absorption mobility-procedure extracts, aqueous wastes, ground water Sept. 1994
7471B Mercury in Solid or Semisolid Waste (Manual Cold-Vapor Technique) Determinative Mercury (Hg) 7439-97-6 Cold- vapor Atomic Absorption soils, sediments, bottom deposits, sludge materials Feb. 2007
7472 Mercury in Aqueous Samples and Extracts by Anodic Stripping Voltammetry (ASV) Determinative Mercury (Hg) 7439-97-6 Anodic Stripping Voltammetry (ASV) drinking water, natural surface water, seawater, domestic/industrial wastewater, soil extracts Dec. 1996
7473 Mercury in Solids and Solutions by Thermal Decomposition, Amalgamation, and Atomic Absorption Spectrophotometry Determinative Mercury (Hg) 7439-97-6 Thermal Decomposition and Atomic Absorption Spectrophotometry (AAS) solids, aqueous samples, digested solutions Feb. 2007
7474 Mercury in Sediment and Tissue Samples by Atomic Fluorescence Spectrometry Determinative Mercury (Hg) 7439-97-6 atomic fluorescence spectrometry (AFS) sediment, tissue Feb. 2007
7580 White Phosphorus (P4) by Solvent Extraction and Gas Chromatography Determinative White Phosphorus (P4) 7723-14-0 Solvent Extraction, Gas Chromatography (GC) soil, sediment, water Dec. 1996
7741A Selenium (Atomic Absorption, Gaseous Hydride) Determinative Selenium (Se) 7782-49-2 atomic absorption spectroscopy (AAS), gaseous hydride wastes, mobility procedure extracts, soils, ground water Sept. 1994
7742 Selenium (Atomic Absorption, Borohydride Reduction) Determinative Selenium (Se) 7782-49-2 atomic absorption spectroscopy (AAS), borohydride reduction wastes, mobility procedure extracts, soils, ground water Sept. 1994
8000D Determinative Chromatographic Separations determinative guidance Perchlorate, white phosphorus (P4), ethylene dibromide (EDB), dibromochloropropane (DBCP), nonhalogenated volatiles, volatiles, acrylonitrile, acrylamide, acetonitrile, phenols, phthalates, nitrosamines, organochlorine pesticides, polychlorinated biphenyls (PCBs), nitroaromatics, cyclic ketones, polynuclear aromatic hydrocarbons (PAHs), haloethers, chlorinated hydrocarbons, aniline & derivatives, organophosphorus pesticides, acid herbicides, semivolatiles, toxaphene and congeners, dioxins, dibenzofurans, carbonyl compounds, acrolein, n-methyl carbamates, nonvolatiles, nitramines, tetrazene, nitroglycerine, bis(2-chloroethyl)ether hydrolysis products NA chromatography NA July 2014
8011 1,2-Dibromoethane and 1,2-Dibromo-3-chloropropane by Microextraction and Gas Chromatography Determinative 1,2-dibromethane, 1,2-dibromo-3-chloropropane 106-93-4, 96-12-8 microextraction, Gas chromatography (GC) ground water, drinking water July 1992
8015C Nonhalogenated Organics by Gas Chromatography Determinative nonhalogenated volatiles and semi volatile organic compounds: Acetone, Acetonitrile, Acrolein, Acrylonitrile, Allyl alcohol, t-Amyl alcohol (TAA), t-Amyl ethyl ether (TAEE), t-Amyl methyl ether (TAME), Benzene, t-Butyl alcohol (TBA), Crotonaldehyde, Diethyl ether, Diisopropyl ether (DIPE), Ethanol, Ethyl acetate, Ethyl benzene, Ethylene oxide, Ethyl tert-butyl ether (ETBE), Isopropyl alcohol (2-Propanol), Methanol, Methyl ethyl ketone (MEK, 2-Butanone), Methyl tert-butyl ether (MTBE), N-Nitroso-di-n-butylamine, Paraldehyde, 2-Pentanone, 2-Picoline, 1-Propanol (n-Propyl alcohol), Propionitrile (Ethyl cyanide), Pyridine, Toluene, o-Toluidine, o-Xylene, m-Xylene, p-Xylene, triethylamine, gasoline range organics (GRO), diesel range organics (DRO) 67-64-1, 75-05-8, 107-02-8, 107-13-1, 107-18-6, 75-85-4, 919-94-8, 994-05-8, 71-43-2, 75-65-0, 123-73-9, 60-29-7, 108-20-3, 64-17-5, 141-78-6, 100-41-4, 75-21-8, 637-92-3, 67-63-0, 67-56-1, 78-93-3, 1634-04-4, 924-16-3, 123-63-7, 107-87-9, 109-06-8, 71-23-8, 107-12-0, 110-86-1, 108-88-3, 95-53-4, 95-47-6, 108-38-3, 106-42-3, 121-44-8 Gas chromatography (GC) water, aqueous wastes, extracts Feb. 2007
8021B Aromatic and Halogenated Volatiles by Gas Chromatography Using Photoionization and/or Electrolytic Conductivity Detectors Determinative aromatic and halogenated volatiles: Allyl chloride, Benzene, Benzyl chloride, Bis(2-chloro-1-methylethyl)ether, Bromoacetone, Bromobenzene, Bromochloromethane, Bromodichloromethane, Bromoform, Bromomethane, Carbon tetrachloride, Chlorobenzene, Chlorodibromomethane, Chloroethane, 2-Chloroethanol, 2-Chloroethyl vinyl ether, Chloroform, Chloromethyl methyl ether, Chloroprene, Chloromethane, 4-Chlorotoluene, 1,2-Dibromo-3-chloropropane, 1,2-Dibromoethane, Dibromomethane, 1,2-Dichlorobenzene, 1,3-Dichlorobenzene, 1,4-Dichlorobenzene, Dichlorodifluoromethane, 1,1-Dichloroethane, 1,2-Dichloroethane, 1,1-Dichloroethene, cis-1,2-Dichloroethene, trans-1,2-Dichloroethene, 1,2-Dichloropropane, 1,3-Dichloro-2-propanol, cis-1,3-dichloropropene, trans-1,3-dichloropropene, Epichlorhydrin, Ethylbenzene, Hexachlorobutadiene, Methylene chloride, Naphthalene, Styrene, 1,1,1,2-Tetrachloroethane, 1,1,2,2-Tetrachloroethane, Tetrachloroethene, Toluene, 1,2,4-Trichlorobenzene, 1,1,1-Trichloroethane, 1,1,2-Trichloroethane, Trichloroethene, Trichlorofluoromethane, 1,2,3-Trichloropropane, Vinyl chloride, o-Xylene, m-Xylene, p-Xylene 107-05-1, 71-43-2, 100-44-7, 108-60-1, 598-31-2, 108-86-1, 74-97-5, 75-27-4, 75-25-2, 74-83-9, 56-23-5, 108-90-7, 124-48-1, 75-00-3, 107-07-03, 110-75-8, 67-66-3, 107-30-2, 126-99-8, 74-87-3, 106-43-4, 96-12-8, 106-93-4, 74-95-3, 95-50-1, 541-73-1, 106-46-7, 75-71-8, 75-34-3, 107-06-2, 75-35-4, 156-59-2, 156-60-5, 78-87-5, 96-23-1, 96-23-1, 10061-02-6, 106-89-8, 100-41-4, 87-68-3, 75-09-2, 91-20-3, 100-42-5, 630-20-6, 79-34-5, 127-18-4, 108-88-3, 120-82-1, 71-55-6, 79-00-5, 79-01-6, 75-69-4, 96-18-4, 75-01-4, 95-47-6, 108-38-3, 106-42-3 Gas chromatography (GC) with photoionization, electrolytic conductivity detection ground water, aqueous sludges, caustic liquors, acid liquors, waste solvents, oily wastes, mousses, tars, fibrous wastes, polymeric emulsions, filter cakes, spent carbons, spent catalysts, soils, sediments July 2014
8031 Acrylonitrile by Gas Chromatography Determinative acrylonitrile 107-13-1 Gas chromatography (GC) with nitrogen–phosphorus detection water Sept. 1994
8032A Acrylamide by Gas Chromatography Determinative acrylamide 79-06-1 Gas chromatography (GC) with electron capture detection aqueous matrices Dec. 1996
8033 Acetonitrile by Gas Chromatography with Nitrogen-Phosphorus Detection Determinative acetonitrile 75-05-8 Gas chromatography (GC) with nitrogen–phosphorus detection aqueous matrices Dec. 1996
8041A Phenols by Gas Chromatography Determinative phenols: 4-Chloro-3-methylphenol, 2-Chlorophenol, 2,4-Dichlorophenol, 2,6-Dichlorophenol, 2,4-Dimethylphenol, 2,4-Dinitrophenol, Dinoseb (2-sec-Butyl-4,6-dinitro phenol), 2-Methyl-4,6-dinitrophenol, 2-Methylphenol (o-Cresol), 3-Methylphenol (m-Cresol), 4-Methylphenol (p-Cresol), 4-Nitrophenol, Pentachlorophenol, Phenol, 2,3,4,6-Tetrachlorophenol, 2,4,5-Trichlorophenol, 2,4,6-Trichlorophenol, 2-Chloro-5-methylphenol, 4-Chloro-2-methylphenol, 3-Chlorophenol, 4-Chlorophenol, 2-Cyclohexyl-4,6-dinitrophenol, 2,3-Dichlorophenol, 2,5-Dichlorophenol, 3,4-Dichlorophenol, 3,5-Dichlorophenol, 2,3-Dimethylphenol, 2,5-Dimethylphenol, 2,6-Dimethylphenol, 3,4-Dimethylphenol, 2,5-Dinitrophenol, 2-Nitrophenol, 3-Nitrophenol, 2,3,4,5-Tetrachlorophenol, 2,3,5,6-Tetrachlorophenol, 2,3,4-Trichlorophenol, 2,3,5-Trichlorophenol, 2,3,6-Trichlorophenol 59-50-7, 95-57-, 120-83-2, 87-65-0, 105-67-9 , 51-28-5, 88-85-7, 534-52-1 , 95-48-7, 108-39-4, 106-44-5, 100-02-7, 87-86-5, 108-95-2, 58-90-2, 95-95-4, 88-06-2, 615-74-7, 1570-64-5, 108-43-0, 106-48-9, 131-89-5, 576-24-9, 583-78-8, 95-77-2, 591-35-5, 526-75-0, 95-87-4, 576-26-1, 95-65-8, 329-71-5, 88-75-5, 554-84-7, 4901-51-3, 935-95-5, 15950-66-0, 933-78-8, 933-75-5 Gas chromatography (GC) sample extracts Feb. 2007
8061A Phthalate Esters by Gas Chromatography with Electron Capture Detection (GC/ECD) Determinative phthalate esters: Benzyl benzoate (Int. Std.), Bis(2-ethylhexyl) phthalate, Butyl benzyl phthalate, Di-n-butyl phthalate, Diethyl phthalate, Dimethyl phthalate, Di-n-octyl phthalate, Bis(2-n-butoxyethyl) phthalate, Bis(2-ethoxyethyl) phthalate, Bis(2-methoxyethyl) phthalate, Bis(4-methyl-2-pentyl) phthalate, Diamyl phthalate, Dicyclohexyl phthalate, Dihexyl phthalate, Diisobutyl phthalate, Dinonyl phthalate, Hexyl 2-ethylhexyl phthalate 120-51-4, 117-81-7, 85-68-7, 84-74-2, 84-66-2, 131-11-3, 117-84-0, 117-83-9, 605-54-9, 117-82-8, 146-50-9, 131-18-0, 84-61-7, 84-75-3, 84-69-5, 84-76-4, 75673-16-4 Gas chromatography (GC) with electron capture detection (ECD) groundwater, leachate, soil, sludge, sediment Dec. 1996
8070A Nitrosamines by Gas Chromatography Determinative nitrosamines: N-Nitrosodimethylamine, N-Nitrosodiphenylamine, N-Nitrosodi-n-propylamine, 62-75-9, 86-30-6, 621-64-7 Gas chromatography (GC) groundwater, municipal discharge, industrial discharge, soils, sediments, sludges Dec. 1996
8081B Organochlorine Pesticides by Gas Chromatography Determinative organochlorine pesticides: Aldrin, ?-BHC, ?-BHC, ?-BHC (Lindane), ?-BHC, cis-Chlordane, trans-Chlordane, Chlordane -- not otherwise specified (n.o.s.), Chlorobenzilate, 1,2-Dibromo-3-chloropropane (DBCP), 4,4'-DDD, 4,4'-DDE, 4,4'-DDT, Diallate, Dieldrin, Endosulfan I, Endosulfan II, Endosulfan sulfate, Endrin, Endrin aldehyde, Endrin ketone, Heptachlor, Heptachlor epoxide, Hexachlorobenzene, Hexachlorocyclopentadiene, Isodrin, Methoxychlor, Toxaphene 309-00-2, 319-84-6, 319-85-7, 58-89-9, 319-86-8, 5103-71-9, 5103-74-2, 57-74-9, 510-15-6, 96-12-8, 72-54-8, 72-55-9, 50-29-3, 2303-16-4, 60-57-1, 959-98-8, 33213-65-9, 1031-07-8, 72-20-8, 7421-93-4, 53494-70-5, 76-44-8, 1024-57-3, 118-74-1, 77-47-4, 465-73-6, 72-43-5, 8001-35-2 Gas chromatography (GC) with electron capture detection (ECD) or electrolytic conductivity detection (ELCD) solid matrices, liquid matrices Feb. 2007
8082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography Determinative Polychlorinated Biphenyl (PCB) Aroclors and congeners: Aroclor 1016, aroclor 1221, aroclor 1232, aroclor 1242, aroclor 1248, aroclor 1252, aroclor 1260, 2-Chlorobiphenyl, 2,3-Dichlorobiphenyl, 2,2',5-Trichlorobiphenyl, 2,4',5-Trichlorobiphenyl, 2,2',3,5'-Tetrachlorobiphenyl, 2,2',5,5'-Tetrachlorobiphenyl, 2,3',4,4'-Tetrachlorobiphenyl, 2,2',3,4,5'-Pentachlorobiphenyl, 2,2',4,5,5'-Pentachlorobiphenyl, 2,3,3',4',6-Pentachlorobiphenyl, 2,2',3,4,4',5'-Hexachlorobiphenyl, 2,2',3,4,5,5'-Hexachlorobiphenyl, 2,2',3,5,5',6-Hexachlorobiphenyl, 2,2',4,4',5,5'-Hexachlorobiphenyl, 2,2',3,3',4,4',5-Heptachlorobiphenyl, 2,2',3,4,4',5,5'-Heptachlorobiphenyl, 2,2',3,4,4',5',6-Heptachlorobiphenyl, 2,2',3,4',5,5',6-Heptachlorobiphenyl, 2,2',3,3',4,4',5,5',6-Nonachlorobiphenyl 12674-11-2, 11104-28-2, 11141-16-5, 53469-21-9, 12672-29-6, 11097-69-1, 11096-82-5, 2051-60-7, 16605-91-7, 37680-65-2, 16606-02-3, 41464-39-5, 35693-99-3, 32598-10-0, 38380-02-8, 37680-73-2, 38380-03-9, 35065-28-2, 52712-04-6, 52663-63-5, 35065-27-1, 35065-30-6, 35065-29-3, 52663-69-1, 52663-68-0, 40186-72-9 Gas chromatography (GC) solid matrices, aqueous matrices, tissue, oils, wipe samples Feb. 2007
8085 Compound-independent Elemental Quantitation of Pesticides by Gas Chromatography with Atomic Emission Detection (GC/AED) Determinative pesticides: Abate (Temephos), Acifluorfen, Alachlor, Aldrin, Ametryn, Atraton, Atrazine, Azinphos ethyl (Ethyl guthion), Azinphos methyl (Guthion), Benfluralin, alpha-BHC, beta-BHC, delta-BHC, gamma-BHC (Lindane), Bromacil, Bromoxynil (Brominal), Butachlor, Butylate, Captafol, Captan, Carbophenothion, Carboxin, trans-Chlordane, Chlorpropham, Chlorpyrifos, Chlorthalonil (Daconil), Coumaphos, Cyanazine, Cycloate, 2,4-D acid, 2,4-DB acid, DCPA (Dacthal), 2,4'-DDD, 4,4'-DDD, 2,4'-DDE, 4,4'-DDE, 2,4'-DDT, 4,4'-DDT, DEF (Butifos), Demeton-O, Demeton-S, Diallate, Diazinon, Dicamba, Dichlobenil (Casoron), 3,5-Dichlorobenzoic acid, Dichlorprop, Dichlorvos (DDVP), Diclofol (Kelthane), Diclofop-methyl, Dieldrin, Dimethoate, Dinoseb, Dioxathion, Diphenamid, Disulfoton (Disyston), Diuron, Endosulfan I, Endosulfan II, Endosulfan sulfate, Endrin, Endrin aldehyde, Endrin ketone, EPN, Eptam (EPTC), Ethalfluralin (Sonalan), Ethion, Ethoprop, Fenamiphos, Fenarimol, Fenitrothion, Fensulfothion, Fenthion, Fluridone, Fonofos, Gardona (Tetrachlovinphos), Heptachlor, Heptachlor epoxide, Hexachlorobenzene, Hexachlorocyclopentadiene, Hexazinone, Imidan (Phosmet), Ioxynil, Malathion, MCPA acid, MCPP acid, Merphos, Metalaxyl, Methoxychlor, Methyl chlorpyrifos, Methyl paraoxon, Methyl parathion, Metolachlor, Metribuzin, Mevinphos, MGK-264, Mirex, Molinate, Napropamide, Norflurazon, 4-Nitrophenol, Oxyfluorfen, Parathion, Pebulate, Pendimethalin, Pentachlorophenol (PCP), Phorate, Phosphamidon, Picloram, Profluralin, Prometon (Pramitol 5p), Prometryn, Pronamide (Kerb), Propachlor (Ramrod), Propargite (S-181), Propazine, Propetamidophos, Ronnel, Silvex (2,4,5-TP), Simazine, Sulfotepp, Sulprofos (Bolstar), 2,4,5-T acid, 2,4,5-TB, Tebuthiuron, Terbacil, Terbutryn (Igran), 2,3,4,5-Tetrachlorophenol, 2,3,4,6-Tetrachlorophenol, Triademefon, Triallate, Triclopyr (Garlon), 2,4,5-Trichlorophenol, 2,4,6-Trichlorophenol, Trifluralin (Treflan), Vernolate 3383-96-13, 62476-59-9, 15972-60-8, 309-00-2, 834-12-8, 1610-17-9, 1912-24-9, 642-71-9, 86-50-0, 1861-40-1, 319-84-6, 319-85-7, 319-86-8, 58-89-9, 314-40-9, 1689-84-5, 23184-66-9, 2008-41-5, 2425-06-1, 133-06-2, 786-19-6, 5234-68-5, 5103-74-2, 101-21-3, 5598-13-0, 1897-45-6, 56-72-4, 21725-46-2, 1134-23-2, 94-75-7, 94-82-6, 2136-79-0, 53-19-0, 72-54-8, 3424-82-6, 72-55-9, 789-02-6, 50-29-3, 78-48-8, 298-02-3, 126-75-0, 2303-16-4, 333-41-5, 1918-00-9, 1194-65-6, 51-36-5, 120-36-5, 62-73-7, 115-32-2, 51338-27-3, 60-57-1, 60-51-5, 88-85-7, 78-34-2, 957-51-7, 298-04-4, 330-54-1, 959-98-8, 33213-65-9, 1031-07-8, 72-20-8, 7421-93-4, 53494-70-5, 2104-64-5, 759-94-4, 55283-68-6, 563-12-2, 13194-48-4, 22224-92-6, 60168-88-9, 122-14-5, 115-90-2, 55-38-9, 59756-60-4, 944-22-9, 961-11-5, 76-44-8, 1024-57-3, 118-74-1, 77-47-4, 51235-04-2, 732-11-6, 1689-83-4, 121-75-5, 94-74-6, 7085-19-0, 150-50-5, 57837-19-1, 72-43-5, 5598-13-0, 311-45-5, 298-00-0, 51218-45-2, 21087-64-9, 7786-34-7, 113-48-4, 2385-85-5, 2212-67-1, 15299-99-7, 27314-13-2, 100-02-7, 42874-03-3, 56-38-2, 1114-71-2, 40487-42-1, 87-86-5, 298-02-2, 297-99-4, 1918-02-1, 26399-36-0, 1610-18-0, 7287-19-6, 23950-58-5, 1918-16-7, 2312-35-8, 139-40-2, 31218-83-4, 299-84-3, 93-76-5, 122-34-9, 3689-24-5, 35400-43-2, 94-82-6, 93-80-1, 34014-18-1, 5902-51-2, 886-50-0, 4901-51-3, 58-90-2, 43121-43-3, 2303-17-5, 55335-06-3, 95-95-4, 88-06-2, 1582-09-8, 1929-77-7 Gas Chromatography with Atomic Emission Detection (GC/AED) liquid matrices, solid matrices Feb. 2007
8091 Nitroaromatics and Cyclic Ketones by Gas Chromatography Determinative 1,4-Dinitrobenzene, 2,4-Dinitrotoluene, 2,6-Dinitrotoluene, 1,4-Naphthoquinone, Nitrobenzene, Pentachloronitrobenzene, Benefin, Butralin, 1-Chloro-2,4-dinitrobenzene, 1-Chloro-3,4-dinitrobenzene, 1-Chloro-2-nitrobenzene, 1-Chloro-4-nitrobenzene, 2-Chloro-6-nitrotoluene, 4-Chloro-2-nitrotoluene, 4-Chloro-3-nitrotoluene, 2,3-Dichloronitrobenzene, 2,4-Dichloronitrobenzene, 3,5-Dichloronitrobenzene, 3,4-Dichloronitrobenzene, 2,5-Dichloronitrobenzene, Dinitramine, 1,2-Dinitrobenzene, 1,3-Dinitrobenzene, Isopropalin, 1,2-Naphthoquinone, 2-Nitrotoluene, 3-Nitrotoluene, 4-Nitrotoluene, Penoxalin (Pendimethalin), Profluralin, 2,3,4,5-Tetrachloronitrobenzene, 2,3,5,6-Tetrachloronitrobenzene, 1,2,3-Trichloro-4-nitrobenzene, 1,2,4-Trichloro-5-nitrobenzene, 2,4,6-Trichloronitrobenzene, Trifluralin 100-25-4, 121-14-2, 606-20-2, 130-15-4, 98-95-3, 82-68-8, 1861-40-1, 33629-47-9, 97-00-7, 610-40-2, 88-73-3, 100-00-5, 83-42-1, 89-59-8, 89-60-1, 3209-22-1, 611-06-3, 618-62-2, 99-54-7, 89-61-2, 29091-05-2, 528-29-0, 99-65-0, 33820-53-0, 524-42-5, 88-72-2, 99-08-1, 99-99-0, 40487-42-1, 26399-36-0, 879-39-0, 117-18-0, 17700-09-3, 89-69-0, 18708-70-8, 1582-09-8 Gas chromatography (GC) with electron capture detection (ECD) or nitrogen-phosphorus detection (NPD) water, soil, waste Dec. 1996
8095 Explosives by Gas Chromatography Determinative explosives: 2-Amino-4,6-dinitrotoluene, 4-Amino-2,6-dinitrotoluene, 3,5-Dinitroaniline, 1,3-Dinitrobenzene, 2,4-Dinitrotoluene, 2,6-Dinitrotoluene, Hexahydro-1,3,5-trinitro-1,3,5-triazine, Nitrobenzene, Nitroglycerine, 2-Nitrotoluene, 3-Nitrotoluene, 4-Nitrotoluene, Octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine, Pentaerythritoltetranitrate, 1,3,5-Trinitrobenzene, 2,4,6-Trinitrophenylmethylnitramine, 2,4,6-Trinitrotoluene 35572-78-2, 1946-51-0, 618-87-1, 99-65-0, 121-14-2, 606-20-2, 121-82-4, 98-95-3, 55-63-0, 88-72-2, 99-08-1, 99-99-0, 2691-41-0, 78-11-5, 99-35-4, 479-45-8, 118-96-7 Gas chromatography (GC) with electron capture detection (ECD) water, soil Feb. 2007
8100 Polynuclear Aromatic Hydrocarbons Determinative Polynuclear Aromatic Hydrocarbons (PAHs): Acenaphthene, acenaphthylene, anthracene, benz(a)anthracene, Benzo(a)pyrene, benzo(b)fluoranthene, benzo(j)fluoranthene, benzo(k)fluoranthene, benzo(g,h,i)perylene, chrysene, dibenzo(a,h)acridine, Dibenz(a,j)acridine, Dibenzo(a,h)anthracene, 7H-Dibenzo(c,g)carbazole, Dibenzo(a,e)pyrene, ibenzo(a,h)pyrene, Dibenzo(a,i)pyrene, Fluoranthene, Fluorene, Indeno(1,2,3-cd)pyrene, 3-Methylcholanthrene, Naphthalene, Phenanthrene, Pyrene 83-32-9, 208-96-8, 120-12-7, 56-55-3, 50-32-8, 205-99-2, 205-82-3, 207-08-9, 191-24-2, 218-01-9, 226-36-8, 224-42-0, 53-70-3, 194-59-2, 192-65-4, 189-64-0, 189-55-9, 206-44-0, 86-73-7, 193-39-5, 56-49-5, 91-20-3, 85-01-8, 129-00-0 Gas chromatography (GC) waste Sept. 1986
8111 Haloethers by Gas Chromatography Determinative haloethers: Bis(2-chloroethoxy)methane, Bis(2-chloroethyl) ether, Bis(2-chloro-1-methylethyl)ether, 4-Chlorophenyl phenyl ether, 4-Bromophenyl phenyl ether, 2-Chlorophenyl 4-nitrophenyl ether, 3-Chlorophenyl 4-nitrophenyl ether, 4-Chlorophenyl 4-nitrophenyl ether, 2,4-Dibromophenyl 4-nitrophenyl ether, 2,4-Dichlorophenyl 3-methyl-4-nitrophenyl ether, 2,6-Dichlorophenyl 4-nitrophenyl ether, 3,5-Dichlorophenyl 4-nitrophenyl ether, 2,5-Dichlorophenyl 4-nitrophenyl ether, 2,4-Dichlorophenyl 4-nitrophenyl ether, 2,3-Dichlorophenyl 4-nitrophenyl ether, 3,4-Dichlorophenyl 4-nitrophenyl ether, 4-Nitrophenyl phenyl ether, 2,4,6-Trichlorophenyl 4-nitrophenyl ether, 2,3,6-Trichlorophenyl 4-nitrophenyl ether, 2,3,5-Trichlorophenyl 4-nitrophenyl ether, 2,4,5-Trichlorophenyl 4-nitrophenyl ether, 3,4,5-Trichlorophenyl 4-nitrophenyl ether, 2,3,4-Trichlorophenyl 4-nitrophenyl ether 111-91-1, 111-44-4, 108-60-1, 7005-72-3, 101-55-3, 209-61-4, 2303-23-3, 1836-74-4, 2671-93-4, 42488-57-3, 2093-28-9, 391-48-7, 1836-75-5, 82239-20-1, 22532-80-5, 620-88-2, 1836-77-7, 22532-68-9 Gas chromatography (GC) water, soil, waste July 2014
8121 Chlorinated Hydrocarbons by Gas Chromatography: Capillary Column Technique Determinative chlorinated hydrocarbons: Benzal chloride, Benzotrichloride, Benzyl chloride, 2-Chloronaphthalene, 1,2-Dichlorobenzene, 1,3-Dichlorobenzene, 1,4-Dichlorobenzene, Hexachlorobenzene, Hexachlorobutadiene, ?-Hexachlorocyclohexane ( ?-BHC), ?-Hexachlorocyclohexane ( ? -BHC), ?-Hexachlorocyclohexane ( ?-BHC), ? -Hexachlorocyclohexane ( ?-BHC), Hexachlorocyclopentadiene, Hexachloroethane, Pentachlorobenzene, 1,2,3,4-Tetrachlorobenzene, 1,2,4,5-Tetrachlorobenzene, 1,2,3,5-Tetrachlorobenzene, 1,2,4-Trichlorobenzene, 1,2,3-Trichlorobenzene, 1,3,5-Trichlorobenzene 98-87-3, 98-07-7, 100-44-7, 91-58-7, 95-50-1, 541-73-1, 106-46-1, 118-74-1, 87-68-3, 319-84-6, 319-85-7, 58-89-9, 319-86-8, 77-47-4, 67-72-1, 608-93-5, 634-66-2, 95-94-2, 634-90-2, 120-82-1, 108-70-3 Gas chromatography (GC) : capillary column water, soil, waste Sept. 1986
8131 Aniline and Selected Derivatives by Gas Chromatography Determinative Aniline, 4-Bromoaniline, 2-Bromo-6-chloro-4-nitroaniline, 2-Bromo-4,6-dinitroaniline, 2-Chloroaniline, 3-Chloroaniline, 4-Chloroaniline , 2-Chloro-4,6-dinitroaniline, 2-Chloro-4-nitroaniline, 4-Chloro-2-nitroaniline, 2,6-Dibromo-4-nitroaniline, 3,4-Dichloroaniline, 2,6-Dichloro-4-nitroaniline, 2,4-Dinitroaniline, 2-Nitroaniline, 3-Nitroaniline, 4-Nitroaniline, 2,4,6-Trichloroaniline, 2,4,5-Trichloroaniline 62-53-3, 106-40-1, 99-29-6, 1817-73-8, 95-51-2, 108-42-9, 106-47-8, 3531-19-9, 121-87-9, 89-63-4, 827-94-1, 95-76-1, 99-30-9, 97-02-9, 88-74-4, 99-09-2, 100-01-6, 634-93-5, 636-30-6 Gas chromatography (GC) aqueous matrices, sample and waste extracts Dec. 1996
8141B Organophosphorus Compounds by Gas Chromatography Determinative Organophosphorus compounds: Asponb, Azinphos-ethyla, Azinphos-methyl, Bolstar (Sulprofos), Carbophenothiona, Chlorfenvinphosa, Chlorpyrifos, Chlorpyrifos methyl, Coumaphos, Crotoxyphosa, Demeton-Oc, Demeton-Sc, Diazinon, Dichlorofenthion, Dichlorvos (DDVP), Dicrotophosa, Dimethoate, Dioxathion, Disulfoton, EPN, Ethion, Ethoprop, Famphur, Fenitrothion, Fensulfothion, Fenthion, Fonophos, Leptophos, Malathion, Merphos, Mevinphos, Monocrotophos, Naled, Parathion, ethyl, Parathion, methyl, Phorate, Phosmet, Phosphamidon, Ronnel, Stirophos (Tetrachlorvinphos, Gardona), Sulfotepp, Tetraethyl pyrophosphate (TEPP), Terbufos, Thionazin (Zinophos), Tokuthion (Prothiofos), Trichlorfon, Trichloronate, Hexamethyl phosphoramide (HMPA), Tri-o-cresyl phosphate (TOCP), Atrazinea, Simazinea, Bendiocarb, Butylate, EPTC, Methiocarb, Molinate, Pebulate, o-Phenylenediamine, Propham, Prosulfocarb, Triallate 3244-90-4, 2642-71-9, 86-50-0, 35400-43-2, 786-19-6, 470-90-6, 2921-88-2, 5598-13-0, 56-72-4, 7700-17-6, 8065-48-3, 8065-48-3, 333-41-5, 97-17-6, 62-73-7, 141-66-2, 60-51-5, 78-34-2, 298-04-4, 2104-64-5, 563-12-2, 13194-48-4, 52-85-7, 122-14-5, 115-90-2, 55-38-9, 944-22-9, 21609-90-5, 121-75-5, 150-50-5, 7786-34-7, 6923-22-4, 300-76-5, 56-38-2, 298-00-0, 298-02-2, 732-11-6, 13171-21-6, 299-84-3, 22248-79-9, 3689-24-5, 107-49-3, 13071-79-9, 297-97-2, 34643-46-4, 52-68-6, 327-98-0, 680-31-9, 78-30-8, 1912-24-9, 122-34-9, 22781-23-3, 2008-41-5, 759-94-4, 2032-65-7, 2212-67-1, 1114-71-2, 95-54-5, 122-42-9, 52888-80-9, 2303-17-5 Gas chromatography (GC) with flame photometric detection (FPD) or nitrogen-phosphorus detection (NPD) liquids, solids Feb. 2007
8151A Chlorinated Herbicides by GC Using Methylation or Pentafluorobenzylation Derivatization Determinative chlorinated acid herbicides: 2,4-D, 2,4-DB, 2,4,5-TP (Silvex), 2,4,5-T, Dalapon, Dicamba, Dichloroprop, Dinoseb, MCPA, MCPP, 4-Nitrophenol, Pentachlorophenol, Acifluorfen, Bentazon, Chloramben, DCPA diacid, 3,5-Dichlorobenzoic acid, 5-Hydroxydicamba, Picloram 94-75-7, 94-82-6, 93-72-1, 93-76-5, 75-99-0, 1918-00-9, 120-36-5, 88-85-7, 94-74-6, 93-65-2, 100-02-1, 87-86-5, 50594-66-6, 25057-89-0, 133-90-4, 2136-79-0, 51-36-5, 7600-50-2, 1918-02-1 Gas chromatography (GC) with electron capture detection (ECD) water, soils, wastes Dec. 1996
8260D Volatile Organic Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) Determinative Volatile Organic Compounds (VOCs): Acetone, Acetonitrile, Acrolein (Propenal), Acrylonitrile, Allyl alcohol, Allyl chloride, t-Amyl ethyl ether (TAEE, 4,4-Dimethyl-3-oxahexane), t-Amul methyl ether (TAME), Benzene, Benzyl chloride, Bromoacetone, Bromobenzene, Bromochloromethane, Bromodichloromethane, Bromoform, Bromomethane, n-Butanol, 2-Butanone (MEK), t-Butyl alcohol, n-Butylbenzene, sec-Butylbenzene, tert-Butylbenzene, Carbon disulfide, Carbon tetrachloride, Chloral hydrate, Chlorobenzene, 1-Chlorobutane, Chlorodibromomethane, Chloroethane, 2-Chloroethanol, 2-Chloroethyl vinyl ether, Chloroform, 1-Chlorohexane, Chloromethane, Chloroprene, 2-Chlorotoluene, 4-Chlorotoluene, Crotonaldehyde, Cyclohexane, 1,2-Dibromo-3-chloropropane, 1,2-Dibromoethane, Dibromomethane, 1,2-Dichlorobenzene, 1,3-Dichlorobenzene, 1,4-Dichlorobenzene, cis-1,4-Dichloro-2-butene, trans-1,4-Dichloro-2-butene, Dichlorodifluoromethane, 1,1-Dichloroethane, 1,2-Dichloroethane, 1,1-Dichloroethene (Vinylidene chloride), cis-1,2-Dichloroethene, trans-1,2-Dichloroethene, 1,3-Dichloropropane, 1,2-Dichloropropane, 2,2-Dichloropropane, 1,3-Dichloro-2-propanol, 1,1-Dichloropropene, cis-1,3-Dichloropropene, trans-1,3-Dichloropropene, 1,2,3,4-Diepoxybutane, Diethyl ether, Diisopropyl ether (DIPE), 1,4-Dioxane, Epichlorohydrin, Ethanol, Ethyl acetate, Ethylbenzene, Ethylene oxide, Ethyl methacrylate, Ethyl-t-butyl-ether (ETBE), Hexachlorobutadiene, Hexachloroethane, 2-Hexanone, Iodomethane (Methyl iodide), Isobutyl alcohol, Isopropylbenzene, p-Isopropyltoluene, Malononitrile, Methacrylonitrile, Methanol, Methyl acetate, Methyl acrylate, Methyl methacrylate, Methyl-tert-butyl ether (MTBE), Methylcyclohexane, Methylene chloride (DCM), 4-Methyl-2-pentanone (MIBK), Naphthalene, Nitrobenzene (NB), 2-Nitropropane, N-Nitroso-di-n-butylamine (N-Nitrosodibutylamine), Paraldehyde, Pentachloroethane, Pentafluorobenzene, 2-Pentanone, 2-Picoline, 1-Propanol, 2-Propanol, Propargyl alcohol, $-Propiolactone, Propionitrile (ethyl cyanide), n-Propylamine, n-Propylbenzene, Pyridine, Styrene, 1,1,1,2-Tetrachloroethane, 1,1,2,2-Tetrachloroethane, Tetrachloroethene, Toluene, o-Toluidine, 1,2,3-Trichlorobenzene, 1,2,4-Trichlorobenzene, 1,1,1-Trichloroethane, 1,1,2-Trichloroethane, Trichloroethene (Trichloroethylene), Trichlorofluoromethane, 1,1,2-Trichlorotrifluoroethane, 1,1,1-Trichlorotrifluoroethane, 1,2,3-Trichloropropane, 1,2,3-Trimethylbenzene, 1,2,4-Trimethylbenzene, 1,3,4-Trimethylbenzene, Vinyl acetate, Vinyl chloride, o-Xylene, m-Xylene, p-Xylene 67-64-1, 75-05-8, 107-02-8, 107-13-1, 107-18-6, 107-05-1, 919-94-8, 994-05-8, 71-43-2, 100-44-7, 598-31-2, 108-86-1, 74-97-5, 75-27-4, 75-25-2, 74-83-9, 71-36-3, 78-93-3, 75-65-0, 104-51-8, 135-98-8, 98-06-6, 75-15-0, 56-23-5, 302-17-0, 108-90-7, 109-69-3, 124-48-1, 75-00-3, 107-07-3, 110-75-8, 67-66-3, 544-10-5, 74-87-3, 126-99-8, 95-49-8, 106-43-4, 4170-30-3, 110-82-7, 96-12-8, 106-93-4, 74-95-3, 95-50-1, 541-73-1, 106-46-7, 1476-11-5, 110-57-6, 75-71-8, 75-34-3, 107-06-2, 75-35-4, 156-59-2, 156-60-5, 142-28-9, 78-87-5, 594-20-7, 96-23-1, 563-58-6, 10061-01-5, 10061-02-6, 1464-53-5, 60-29-7, 108-20-3, 123-91-1, 106-89-8, 64-17-5, 141-78-6, 100-41-4, 75-21-8, 97-63-2, 637-92-3, 87-68-3, 67-72-1, 591-78-6, 74-88-4, 78-83-1, 98-82-8, 99-87-6, 109-77-3, 126-98-7, 67-56-1, 79-20-9, 96-33-3, 80-62-6, 1634-04-4, 108-87-2, 75-09-2, 108-10-1, 91-20-3, 98-95-3, 79-46-9, 924-16-3, 123-63-7, 76-01-7, 363-72-4, 107-87-9, 109-06-8, 71-23-8, 67-63-0, 107-19-7, 57-57-8, 107-12-0, 107-10-8, 103-65-1, 110-86-1, 100-42-5, 630-20-6, 79-34-5, 127-18-4, 108-88-3, 2037-26-5, 95-53-4, 87-61-6, 120-82-1, 71-55-6, 79-00-5, 79-01-6, 76-13-1, 354-58-5, 75-69-4, 96-18-4, 526-73-8, 95-63-6, 108-67-8, 108-05-4, 75-01-4, 95-47-6, 108-38-3, 106-42-3 Gas Chromatography/ Mass Spectrometry (GC/MS) air sampling trapping, ground water, surface water, aqueous sludges, caustic liquors, acid liquors, waste solvents, oily wastes, mousses, tars, fibrous wastes, polymeric emulsions, filter cakes, spent carbons, spent catalysts, soils, sediments July 2018
8261 Volatile Organic Compounds by Vacuum Distillation in Combination with Gas Chromatography/Mass Spectrometry (VD/GC/MS) Determinative volatile organic compounds (VOCs): Acetone, Acetonitrile, Acetophenone, Acrolein, Acrylonitrile, Allyl chloride, t-Amyl ethyl ether (TAEE, 4,4-Dimethyl-3-oxahexane), t-Amyl methyl ether (TAME), Aniline, Benzene, Bromochloromethane, Bromodichloromethane, Bromomethane, 2-Butanone, t-Butyl alcohol (TBA), n-Butylbenzene, sec-Butylbenzene, tert-Butylbenzene, Carbon disulfide, Carbon tetrachloride, Chlorobenzene, Chlorodibromomethane, Chloroethane, Chloroform, Chloromethane, 2-Chlorotoluene, 4-Chlorotoluene, 1,2-Dibromo-3-chloropropane, Dibromomethane, 1,2-Dichlorobenzene, 1,3-Dichlorobenzene, 1,4-Dichlorobenzene, cis-1,4-Dichloro-2-butene, trans-1,4-Dichloro-2-butene, Dichlorodifluoromethane, 1,1-Dichloroethane, 1,2-Dichloroethane, 1,1-Dichloroethene, trans-1,2-Dichloroethene, cis-1,2-Dichloroethene, 1,2-Dichloropropane, 1,3-Dichloropropane, 2,2-Dichloropropane, 1,1-Dichloropropene, cis-1,3-Dichloropropene, trans-1,3-Dichloropropene, Diethyl ether, Diisopropyl ether (DIPE), 1,4-Dioxane, Ethanol, Ethyl acetate, Ethylbenzene, Ethyl t-butyl ether (ETBE), Ethyl methacrylate, Hexachlorobutadiene, 2-Hexanone, Iodomethane, Isobutyl alcohol, Isopropylbenzene, p-Isopropyltoluene, Methacrylonitrile, Methyl t-butyl ether (MTBE), Methylene chloride, Methyl methacrylate, 1-Methylnaphthalene, 2-Methylnaphthalene, 4-Methyl-2-pentanone (MIBK), Naphthalene, N-Nitrosodibutylamine, N-Nitrosodiethylamine, N-Nitrosodimethylamine, N-Nitrosodi-n-propylamine, N-Nitrosomethylethylamine, Pentachloroethane, 2-Picoline, Propionitrile, n-Propylbenzene, Pyridine, Styrene, 1,1,2,2-Tetrachloroethane, Tetrachloroethene, Tetrahydrofuran, Toluene, o-Toluidine, 1,2,3-Trichlorobenzene, 1,2,4-Trichlorobenzene, 1,1,1-Trichloroethane, 1,1,2-Trichloroethane, Trichloroethene, Trichlorofluoromethane, 1,2,3-Trichloropropane, 1,2,4-Trimethylbenzene, 1,3,5-Trimethylbenzene, Vinyl chloride, o-Xylene, m-Xylene, p-Xylene 67-64-1, 75-05-8, 98-86-2, 107-02-8, 107-13-1, 107-05-1, 919-94-8, 994-05-8, 62-53-3, 71-43-2, 74-97-5, 75-27-4, 75-25-2, 74-83-9, 78-93-3, 75-65-0, 104-51-8, 135-98-8, 98-06-6, 75-15-0, 56-23-5, 108-90-7, 124-48-1, 75-00-3, 67-66-3, 74-87-3, 95-49-8, 106-43-4, 96-12-8, 74-95-3, 95-50-1, 541-73-1, 106-46-7,764-41-0, 110-57-6,75-71-8, 75-34-3, 107-06-2, 75-35-4, 156-60-5, 156-59-2, 78-87-5, 142-28-9, 594-20-7, 563-58-6, 10061-01-5, 10061-02-6, 60-29-7, 108-20-3, 123-91-1, 64-17-5, 141-78-6, 100-41-4, 637-92-3, 97-63-2, 87-68-3, 591-78-6, 74-88-4, 78-83-1, 98-82-8, 99-87-6, 126-98-7, 1634-04-4, 75-09-2, 80-62-6, 90-12-0, 91-57-6, 108-10-1, 91-20-3, 924-16-3, 55-18-5, 62-75-9, 621-64-7, 10595-95-6, 76-01-7, 109-06-8, 107-12-0, 103-65-1, 110-86-1, 100-42-5, 79-34-5, 127-18-4, 109-99-9, 108-88-3, 95-53-4, 87-61-6, 120-82-1, 71-55-6, 79-00-5, 79-01-6, 75-69-4, 96-18-4, 95-63-6, 108-67-8, 75-01-4, 95-47-6, 108-38-3, 106-42-3 Vacuum Distillation, Gas Chromatography/ Mass Spectrometry (VD/GC/MS) liquid waste, solid waste, oily waste, tissue Feb. 2007
8270E Semivolatile Organic Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) Determinative semivolatile organics: Acenaphthene, Acenaphthylene, Acetophenone, 2-Acetylaminofluorene, 1-Acetyl-2-thiourea, Aldrin, 2-Aminoanthraquinone, Aminoazobenzene, 4-Aminobiphenyl, 3-Amino-9-ethylcarbazole, Anilazine, Aniline, o-Anisidine, Anthracene, Aramite, Aroclor 1016, Aroclor 1221, Aroclor 1232, Aroclor 1242, Aroclor 1248, Aroclor 1254, Aroclor 1260, Atrazine, Azinphos-methyl (Guthion), Azonbenzene, Barban, Benzaldehyde, Benzidine, Benzoic acid, Benz(a)anthracene, Benzo(b)fluoranthene, Benzo(k)fluoranthene, Benzo(g,h,i)perylene, Benzo(a)pyrene, Benzo(e)pyrene, p-Benzoquinone, Benzyl alcohol, alpha-BHC, beta-BHC, delta-BHC, gamma-BHC (Lindane), 1,1'-Biphenyl, Bis(2-chloroethoxy)methane, Bis(2-chloroethyl) ether, Bis(2-chloro-1-methylethyl)ether, Bis(2-ethylhexyl) phthalate, 4-Bromophenyl phenyl ether, Bromoxynil, Butyl benzyl phthalate, Caprolactam, Captafol, Captan, Carbaryl (Sevin), Carbazole, Carbofuran (Furaden), Carbophenothion, Chlordane (NOS), Chlorfenvinphos, 4-Chloroaniline, Chlorobenzilate, 5-Chloro-2-methylaniline, 4-Chloro-3-methylphenol, 3-(Chloromethyl)pyridine hydrochloride, 1-Chloronaphthalene, 2-Chloronaphthalene, 2-Chlorophenol, 4-Chloro-1,2-phenylenediamine, 4-Chloro-1,3-phenylenediamine, 4-Chlorophenyl phenyl ether, Chrysene, Coumaphos, p-Cresidine, Crotoxyphos, 2-Cyclohexyl-4,6-dinitro-phenol, 4,4'-DDD, 4,4'-DDE, 4,4'-DDT, Demeton-O, Demeton-S, Diallate (cis or trans), 2,4-Diaminotoluene, Dibenz(a,j)acridine, Dibenz(a,h)anthracene, Dibenzofuran, Dibenzo(a,e)pyrene, 1,2-Dibromo-3-chloropropane, Di-n-butyl phthalate, Dichlone, 1,2-Dichlorobenzene. 1,3-Dichlorobenzene, 1,4-Dichlorobenzene, 3,3'-Dichlorobenzidine, 2,4-Dichlorophenol, 2,6-Dichlorophenol, Dichlorovos, Dicrotophos, Dieldrin, Diethyl phthalate, Diethylstilbestrol, Diethyl sulfate, Dimethoate, 3,3'-Dimethoxybenzidine, Dimethylaminoazobenzene, 7,12-Dimethylbenz(a)-anthracene, 3,3'-Dimethylbenzidine, alpha,alpha-Dimethylphenethylamine, 2,4-Dimethylphenol, Dimethyl phthalate, 1,2-Dinitrobenzene, 1,3-Dinitrobenzene (1,3-DNB), 1,4-Dinitrobenzene, 4,6-Dinitro-2-methylphenol, 2,4-Dinitrophenol, 2,4-Dinitrotoluene (2,4-DNT), 2,6-Dinitrotoluene (2,6-DNT), Dinocap, Dinoseb (DNBP), 1,4-Dioxane, Diphenylamine, 5,5-Diphenylhydantoin, 1,2-Diphenylhydrazine, Di-n-octyl phthalate, Disulfoton, Endosulfan I, Endosulfan II, Endosulfan sulfate, Endrin, Endrin aldehyde, Endrin ketone, EPN, Ethion, Ethyl carbamate, Ethyl methanesulfonate, Famphur, Fensulfothion, Fenthion, Fluchloralin, Fluoranthene, Fluorene, 2-Fluorobiphenyl (surr), 2-Fluorophenol (surr), Heptachlor, Heptachlor epoxide, Hexachlorobenzene, Hexachlorobutadiene, Hexachlorocyclopentadiene, Hexachloroethane, Hexachlorophene, Hexachloropropene, Hexamethylphosphoramide, Hydroquinone, Indeno(1,2,3-cd)pyrene, Isodrin, Isophorone, Isosafrole, Kepone, Leptophos, Malathion , Maleic anhydride, Mestranol, Methapyrilene, Methoxychlor, 3-Methylcholanthrene, 4,4'-Methylenebis (2-chloroaniline), 4,4'-Methylenebis(N,N-dimethylaniline), 1-Methylnaphthalene, 2-Methylnaphthalene, Methyl parathion, 2-Methylphenol, 3-Methylphenol, 4-Methylphenol, Mevinphos, Mexacarbate, Mirex, Monocrotophos, Naled, Naphthalene, 1,4-Naphthoquinone, 1-Naphthylamine, 2-Naphthylamine, Nicotine, 5-Nitroacenaphthene, 2-Nitroaniline, 3-Nitroaniline, 4-Nitroaniline, 5-Nitro-o-anisidine, Nitrobenzene, 4-Nitrobiphenyl, Nitrofen, 2-Nitrophenol, 4-Nitrophenol, 4-Nitroquinoline-1-oxide, N-Nitrosodi-n-butylamine, N-Nitrosodiethylamine, N-Nitrosodimethylamine, N-Nitrosodiphenylamine, N-Nitrosodi-n-propylamine, N-Nitrosomethylethylamine, N-Nitrosomorpholine, N-Nitrosopiperidine, N-Nitrosopyrrolidine, 5-Nitro-o-toluidine, Octamethyl pyrophosphoramide, 4,4'-Oxydianiline, Parathion, Pentachlorobenzene, Pentachloronitrobenzene, Pentachlorophenol, Perylene, Phenacetin, Phenanthrene, Phenobarbital, Phenol, 1,4-Phenylenediamine, Phorate, Phosalone, Phosmet, Phosphamidon, Phthalic anhydride, 2-Picoline (2-Methylpyridine), Piperonyl sulfoxide, Pronamide, Propylthiouracil, Pyrene, Pyridine, Resorcinol, Safrole, Strychnine, Sulfallate, Terbufos, 1,2,4,5-Tetrachlorobenzene, 2,3,4,6-Tetrachlorophenol, Tetrachlorvinphos, Tetraethyl dithiopyrophosphate, Tetraethyl pyrophosphate, Thionazine, Thiophenol (Benzenethiol), 2,4-Toluene diisocyanate, o-Toluidine, Toxaphene, 1,2,4-Trichlorobenzene, 2,4,5-Trichlorophenol, 2,4,6-Trichlorophenol, Trifluralin, 2,4,5-Trimethylaniline, Trimethyl phosphate, 1,3,5-Trinitrobenzene, Tris(2,3-dibromopropyl) phosphate, Tri-p-tolyl phosphate, O,O,O-Triethyl phosphorothioate 83-32-9, 208-96-8, 98-86-2, 53-96-3, 591-08-2, 309-00-2, 117-79-3, 60-09-3, 92-67-1, 132-32-1, 101-05-3, 62-53-3, 90-04-0, 120-12-7, 140-57-8, 12674-11-2,11104-28-2, 11141-16-5, 53469-21-9, 12672-29-6, 11097-69-1, 11096-82-5, 1912-24-9, 86-50-0, 103-33-3, 101-27-9, 100-52-7, 92-87-5, 65-85-0, 56-55-3, 205-99-2, 207-08-9, 191-24-2, 50-32-8, 192-97-2, 106-51-4,100-51-6, 319-84-6,319-85-7, 319-86-8, 58-89-9, 92-52-4, 111-91-1, 111-44-4,39638-32-9, 117-81-7, 101-55-3, 1689-84-5, 85-68-7, 105-60-2, 2425-06-1, 133-06-2, 63-25-2, 86-74-8, 1563-66-2, 786-19-6, 57-74-9, 470-90-6, 106-47-8, 510-15-6, 95-79-4, 59-50-7, 6959-48-4, 90-13-1, 91-58-7, 95-57-8, 95-83-0, 5131-60-2,7005-72-3, 218-01-9, 56-72-4, 120-71-8, 7700-17-6, 131-89-5, 72-54-8, 72-55-9, 50-29-3, 298-03-3, 126-75-0, 2303-16-4, 95-80-7, 224-42-0, 53-70-3, 132-64-9, 192-65-4, 96-12-8, 84-74-2, 117-80-6, 95-50-1, 541-73-1, 106-46-7, 91-94-1, 120-83-2 , 87-65-0, 62-73-7, 141-66-2, 60-57-1 , 84-66-2, 56-53-1, 64-67-5, 60-51-5, 119-90-4, 60-11-7, 57-97-6, 119-93-7, 122-09-8, 105-67-9, 131-11-3, 528-29-0, 99-65-0, 100-25-4, 534-52-1, 51-28-5, 121-14-2, 606-20-2, 39300-45-3, 88-85-7, 123-91-1, 122-39-4,57-41-0, 122-66-7, 117-84-0, 298-04-4, 959-98-8, 33213-65-9, 1031-07-8, 72-20-8, 7421-93-4, 53494-70-5, 2104-64-5, 563-12-2, 51-79-6, 62-50-0, 52-85-7, 115-90-2, 55-38-9, 33245-39-5, 206-44-0, 86-73-7, 321-60-8, 367-12-4, 76-44-8, 1024-57-3 , 118-74-1, 87-68-3, 77-47-4, 67-72-1, 70-30-4, 1888-71-7, 680-31-9, 123-31-9, 193-39-5, 465-73-6, 78-59-1, 120-58-1, 143-50-0, 55-38-9, 33245-39-5, 206-44-0, 86-73-7, 321-60-8, 367-12-4, 76-44-8, 1024-57-3, 118-74-1, 87-68-3, 77-47-4, 67-72-1,70-30-4, 1888-71-7, 680-31-9, 123-31-9, 193-39-5, 465-73-6, 78-59-1, 120-58-1, 143-50-0, 21609-90-5, 121-75-5, 108-31-6, 72-43-5, 66-27-3, 298-00-0, 56-49-5, 101-14-4, 101-61-1, 90-12-0, 91-57-6, 95-48-7, 108-39-4, 106-44-5, 7786-34-7, 315-18-4, 2385-85-5, 6923-22-4, 300-76-5, 91-20-3, 130-15-4, 134-32-7, 91-59-8, 54-11-5, 602-87-9, 88-74-4, 99-09-2, 100-01-6, 99-59-2, 98-95-3, 92-93-3, 1836-75-5, 88-75-5, 100-02-7, 99-55-8, 56-57-5, 924-16-3, 55-18-5, 62-75-9, 86-30-6, 621-64-7, 10595-95-6, 59-89-2, 100-75-4, 930-55-2, 152-16-9, 101-80-4, 56-38-2, 608-93-5, 82-68-8, 87-86-5, 198-55-0, 62-44-2, 85-01-8, 50-06-6, 108-95-2, 106-50-3, 298-02-2, 2310-17-0, 732-11-6, 13171-21-6, 85-44-9, 109-06-8, 120-62-7, 23950-58-5, 51-52-5, 129-00-0, 110-86-1, 108-46-3, 94-59-7, 57-24-9, 95-06-7, 13071-79-9, 95-94-3, 58-90-2, 961-11-5, 3689-24-5, 107-49-3, 297-97-2, 108-98-5, 584-84-9, 95-53-4, 8001-35-2, 120-82-1, 95-95-4, 88-06-2, 126-68-1, 1582-09-8, 512-56-1, 137-17-7, 99-35-4, 126-72-7, 78-32-0 Gas Chromatography/ Mass Spectrometry (GC/MS) solid waste matrices, soils, air sampling media, water samples July 2018
8275A Semivolatile Organic Compounds (PAHs and PCBs) in Soils/Sludges and Solid Wastes Using Thermal Extraction/Gas Chromatography/Mass Spectrometry (TE/GC/MS) Determinative Polynuclear Aromatic Hydrocarbons (PAHs) and Polychlorinated Biphenyls (PCBs): Acenaphthene, Acenaphthylene, Anthracene, Benz[a]anthracene, Benzo[a]pyrene, Benzo[b]fluoranthene, Benzo[g,h,i]perylene, Benzo[k]fluoranthene, 4-Bromophenyl phenyl ether, 1-Chloronaphthalene, Chrysene, Dibenzofuran, Dibenz[a,h]anthracene, Dibenzothiophene, Fluoranthene, Fluorene, Hexachlorobenzene, Indeno(1,2,3-cd)pyrene, Naphthalene, Phenanthrene, Pyrene, 1,2,4-Trichlorobenzene, 2-Chlorobiphenyl, 3,3'-Dichlorobiphenyl, 2,2',5-Trichlorobiphenyl, 2,3',5-Trichlorobiphenyl, 2,4',5-Trichlorobiphenyl, 2,2',5,5'-Tetrachlorobiphenyl, 2,2',4,5'-Tetrachlorobiphenyl, 2,2',3,5'-Tetrachlorobiphenyl, 2,3',4,4'-Tetrachlorobiphenyl, 2,2',4,5,5'-Pentachlorobiphenyl, 2,3',4,4',5-Pentachlorobiphenyl, 2,2',3,4,4',5'-Hexachlorobiphenyl, 2,2',3,4',5,5',6-Heptachlorobiphenyl, 2,2',3,3',4,4'-Hexachlorobiphenyl, 2,2',3,4,4',5,5'-Heptachlorobiphenyl, 2,2',3,3',4,4',5-Heptachlorobiphenyl, 2,2',3,3',4,4',5,5'-Octachlorobiphenyl, 2,2',3,3',4,4',5,5',6-Nonachlorobiphenyl, 2,2',3,3',4,4',5,5',6,6'-Decachlorobiphenyl 83-32-9, 208-96-8, 120-12-7, 56-55-3, 50-32-8, 205-99-2, 191-24-2, 207-08-9, 101-55-3, 90-13-1, 218-01-9, 132-64-9, 53-70-3, 132-65-0, 206-44-0, 86-73-7, 118-74-1, 193-39-5, 91-20-3, 85-01-8, 129-00-0, 120-82-1, 2051-60-7, 2050-67-1, 37680-65-2, 3844-81-4, 16606-02-3, 35693-99-3, 41464-40-8, 41464-39-5, 32598-10-0, 37680-73-2, 31508-00-6, 35065-28-2, 52663-68-0, 38380-07-3, 35065-29-3, 35065-30-6, 35694-08-7, 40186-72-9, 2051-24-3 Thermal Extraction, Gas Chromatography/ Mass Spectrometry (TE/GC/MS) soil, sludges, solid waste Dec. 1996
8276 Toxaphene and Toxaphene Congeners by Gas Chromatorgraphy/Negative Ion Chemical Ionization Mass Spectrometry (GC-NICI/MS) Determinative Toxaphene, 2-exo,3-endo,6-exo,8,9,10-Hexachlorobornane (Hx-Sed), 2-endo,3-exo,5-endo,6-exo,8,9,10-Heptachlorobornane (Hp-Sed), 2-endo,3-exo,5-endo,6-exo,8,8,10,10-Octachlorobornane (P26), 2-endo,3-exo,5-endo,6-exo,8,9,10,10-Octachlorobornane (P40), 2-exo,3-endo,5-exo,8,9,9,10,10-Octachlorobornane (P41) , 2-exo,5,5,8,9,9,10,10-Octachlorobornane (P44) , 2-endo,3-exo,5-endo,6-exo,8,8,9,10,10-Nonachlorobornane (P50), 2,2,5,5,8,9,9,10,10-Nonachlorobornane (P62) 8001-35-2, Hx-Sed: 57981-29-0, Hp-Sed: 70649-42-2, P26: 142534-71-2, P40: 166021-27-8, P41: 165820-16-6, P44: 165820-17-7, P50: 6680-80-8, P62: 154159-06-5 Gas Chromatorgraphy/Negative Ion Chemical Ionization Mass Spectrometry (GC-NICI/MS) solid & liquid matrices July 2014
8280B Polychlorinated Dibenzo-p-Dioxins (PCDDs) and Polychlorinated Dibenzofurans (PCDFs) by High Resolution Gas Chromatography/Low Resolution Mass Spectrometry (HRGC/LRMS) Determinative Polychlorinated Dibenzo-p-Dioxins (PCDDs) and Polychlorinated Dibenzofurans (PCDFs): 2,3,7,8-Tetrachlorodibenzo-p-dioxin (TCDD), 1,2,3,7,8-Pentachlorodibenzo-p-dioxin (PeCDD), 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin (HxCDD), 1,2,3,6,7,8-Hexachlorodibenzo-p-dioxin (HxCDD), 1,2,3,7,8,9-Hexachlorodibenzo-p-dioxin (HxCDD), 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (HpCDD), 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD), 2,3,7,8-Tetrachlorodibenzofuran (TCDF), 1,2,3,7,8-Pentachlorodibenzofuran (PeCDF), 2,3,4,7,8-Pentachlorodibenzofuran (PeCDF), 1,2,3,4,7,8-Hexachlorodibenzofuran (HxCDF), 1,2,3,6,7,8-Hexachlorodibenzofuran (HxCDF), 1,2,3,7,8,9-Hexachlorodibenzofuran (HxCDF), 2,3,4,6,7,8-Hexachlorodibenzofuran (HxCDF), 1,2,3,4,6,7,8-Heptachlorodibenzofuran (HpCDF), 1,2,3,4,7,8,9-Heptachlorodibenzofuran (HpCDF), 1,2,3,4,5,6,7,8-Octachlorodibenzofuran (OCDF), Total Tetrachlorodibenzo-p-dioxin (TCDD), Total Pentachlorodibenzo-p-dioxin (PeCDD), Total Hexachlorodibenzo-p-dioxin (HxCDD), Total Heptachlorodibenzo-p-dioxin (HpCDD), Total Tetrachlorodibenzofuran (TCDF), Total Pentachlorodibenzofuran (PeCDF), Total Hexachlorodibenzofuran (HxCDF), Total Heptachlorodibenzofuran (HpCDF) 1746-01-6, 40321-76-4, 39227-28-6, 57653-85-7, 19408-74-3, 35822-46-9, 3268-87-9, 51207-31-9, 57117-41-6, 57117-31-4, 70648-26-9, 57117-44-9, 72918-21-9, 60851-34-5, 67562-39-4, 55673-89-7, 39001-02-0, 41903-57-5, 36088-22-9, 34465-46-8, 37871-00-4, 55722-27-5, 30402-15-4, 55684-94-1, 38998-75-3 High Resolution Gas Chromatography/Low Resolution Mass Spectrometry (HRGC/LRMS) water, soil, fly ash, chemical waste samples, fuel oil, sludge Feb. 2007
8290A Polychlorinated Dibenzodioxins (PCDDs) and Polychlorinated Dibenzofurans (PCDFs) by High-Resolution Gas Chromatography/High-Resolution Mass Spectrometry (HRGC/HRMS) Determinative Polychlorinated Dibenzo-p-Dioxins (PCDDs) and Polychlorinated Dibenzofurans (PCDFs): 2,3,7,8-Tetrachlorodibenzo-p-dioxin (TCDD), 1,2,3,7,8-Pentachlorodibenzo-p-dioxin (PeCDD), 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin (HxCDD), 1,2,3,6,7,8-Hexachlorodibenzo-p-dioxin (HxCDD), 1,2,3,7,8,9-Hexachlorodibenzo-p-dioxin (HxCDD), 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (HpCDD), 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD), 2,3,7,8-Tetrachlorodibenzofuran (TCDF), 1,2,3,7,8-Pentachlorodibenzofuran (PeCDF), 2,3,4,7,8-Pentachlorodibenzofuran (PeCDF), 1,2,3,4,7,8-Hexachlorodibenzofuran (HxCDF), 1,2,3,6,7,8-Hexachlorodibenzofuran (HxCDF), 1,2,3,7,8,9-Hexachlorodibenzofuran (HxCDF), 2,3,4,6,7,8-Hexachlorodibenzofuran (HxCDF), 1,2,3,4,6,7,8-Heptachlorodibenzofuran (HpCDF), 1,2,3,4,7,8,9-Heptachlorodibenzofuran (HpCDF), 1,2,3,4,5,6,7,8-Octachlorodibenzofuran (OCDF), Total Tetrachlorodibenzo-p-dioxin (TCDD), Total Pentachlorodibenzo-p-dioxin (PeCDD), Total Hexachlorodibenzo-p-dioxin (HxCDD), Total Heptachlorodibenzo-p-dioxin (HpCDD), Total Tetrachlorodibenzofuran (TCDF), Total Pentachlorodibenzofuran (PeCDF), Total Hexachlorodibenzofuran (HxCDF), Total Heptachlorodibenzofuran (HpCDF) 1746-01-6, 40321-76-4, 39227-28-6, 57653-85-7, 19408-74-3, 35822-46-9, 3268-87-9, 51207-31-9, 57117-41-6, 57117-31-4, 70648-26-9, 57117-44-9, 72918-21-9, 60851-34-5, 67562-39-4, 55673-89-7, 39001-02-0, 41903-57-5, 36088-22-9, 34465-46-8, 37871-00-4, 55722-27-5, 30402-15-4, 55684-94-1, 38998-75-3 High-Resolution Gas Chromatography, High-Resolution Mass Spectrometry (HRGC/HRMS) soil, sediment, fly ash, tissue, sample extracts Feb. 2007
8310 Polynuclear Aromatic Hydrocarbons Determinative Polynuclear Aromatic Hydrocarbons (PAHs): Acenaphthene, Acenaphthylene, Anthracene, Benzo(a)anthracene, Benzo(a)pyrene, Benzo(b)fluoranthene, Benzo(g,h,i)perylene, Benzo(k)fluoranthene, Chrysene, Dibenzo(a,h)anthracene, Fluoranthene, Fluorene, Indeno(1,2,3-cd)pyrene, Naphthalene, Phenanthrene, Pyrene 83-32-9, 208-96-8, 120-12-7, 56-55-3, 50-32-8, 205-99-2, 191-24-2, 207-08-9, 218-01-9, 53-70-3, 206-44-0, 86-73-7, 193-39-5, 91-20-3, 85-01-8, 129-00-0 High Performance Liquid Chromatograph (HPLC) groundwater, wastes Sept. 1986
8315A Determination of Carbonyl Compounds by High Performance Liquid Chromatography (HPLC) determinative carbonyls: Acetaldehyde, Acetone, Acrolein, Benzaldehyde, Butanal (Butyraldehyde), Crotonaldehyde, Cyclohexanone, Decanal, 2,5-Dimethylbenzaldehyde, Formaldehyde, Heptanal, Hexanal (Hexaldehyde), Isovaleraldehyde, Nonanal, Octanal, Pentanal (Valeraldehyde), Propanal (Propionaldehyde), m-Tolualdehyde, o-Tolualdehyde, p-Tolualdehyde 75-07-0, 67-64-1, 107-02-8, 100-52-7, 123-72-8, 123-73-9, 108-94-1, 112-31-2, 5779-94-2, 50-00-0, 111-71-7, 66-25-1, 590-86-3, 124-19-6, 124-13-0, 110-62-3, 123-38-6, 620-23-5, 529-20-4, 104-87-0 High Performance Liquid Chromatograph (HPLC) aqueous samples, soils, waste samples, stack samples Dec. 1996
8316 Acrylamide, Acrylonitrile and Acrolein by High Performance Liquid Chromatography (HPLC) Determinative acrylamide, acrylonitrile, acrolein 79-06-1, 107-13-1, 107-02-8 High Performance Liquid Chromatograph (HPLC) water Sept. 1994
8318A N-Methylcarbamates by High Performance Liquid Chromatography (HPLC) Determinative n-methylcarbamates: Aldicarb (Temik), Aldicarb sulfone, Bendiocarb, Carbaryl (Sevin), Carbofuran (Furadan), m-Cumenyl methylcarbamate, Dioxacarb, Formetanate hydrochloride, 3-Hydroxycarbofuran, Methiocarb (Mesurol), Methomyl (Lannate), Metolcarb, Mexacarbate, Oxamyl, Promecarb, Propoxur (Baygon), Thiodicarb 116-06-3, 1646-88-4, 22781-23-3, 63-25-2, 1563-66-2,64-00-6, 6988-21-2, 23422-53-9, 16655-82-6, 2032-65-7, 16752-77-5, 1129-41-5, 315-18-4, 23135-22-0, 2631-37-0, 114-26-1, 59669-26-0 High Performance Liquid Chromatograph (HPLC) water, aqueous samples, soils, sludges, solids, oily wastes Feb. 2007
8321B Solvent Extractable Nonvolatile Compounds by High Performance Liquid Chromatography/Thermospray/Mass Spectrometry (HPLC/TS/MS) or Ultraviolet(HPLC/TS/MS)Detection Determinative nonvolatiles: Disperse Red 1, Disperse Red 5, Disperse Red 13, Disperse Yellow 5, Disperse Orange 3, Disperse Orange 30, Disperse Brown 1, Solvent Red 3, Solvent Red 23, Disperse Blue 3, Disperse Blue 14, Disperse Red 60, Methomyl, Thiofanox, Famphur, Asulam, Dichlorvos (DDVP), Dimethoate, Disulfoton, Fensulfothion, Merphos, Parathion methyl, Monocrotophos, Naled, Phorate, Trichlorfon, Tris (2,3-dibromopropyl) phosphate (Tris-BP), Dalapon, Dicamba, 2,4-D, MCPA, MCPP, Dichlorprop, 2,4,5-T, Silvex (2,4,5-TP), Dinoseb, 2,4-DB, 2,4-D, butoxyethanol ester, 2,4-D, ethylhexyl ester, 2,4,5-T, butyl ester, 2,4,5-T, butoxyethanol ester, Aldicarb, Aldicarb sulfone, Aldicarb sulfoxide, Aminocarb, Barban, Benomyl, Bendiocarb, Bromacil, Butylate, Carbaryl, Carbendazim, Carbofuran, Carbosulfan, Chloropropham, Chloroxuron, m-Cumenyl methyl carbamate, Diuron, EPTC, Fenuron, Fluometuron, Formetanate hydrochloride, 3-Hydroxycarbofuran, Linuron, Methiocarb, Methomyl, Metolcarb, Mexacarbate, Molinate, Monuron, Neburon, Oxamyl, Pebulate, o-Phenylenediamine, Physostigmine, Physostigmine salicylate, Promecarb, Propham, Propoxur, Prosulfocarb, Siduron, Tebuthiuron 2872-52-8, 3769-57-1, 126038-78-6, 6439-53-8, 730-40-5, 5261-31-4, 17464-91-4, 6535-42-8, 85-86-9, 2475-46-9, 2475-44-7, 17418-58-5, 16752-77-5, 39196-18-4, 52-85-7, 3337-71-1, 62-73-7, 60-51-5, 298-04-4, 115-90-2, 150-50-5, 298-00-0, 6923-22-4, 300-76-5, 298-02-2, 52-68-6, 126-72-7, 75-99-0, 1918-00-9, 94-75-7, 94-74-6, 7085-19-0, 120-36-5, 93-76-5, 93-72-1, 88-85-7, 94-82-6, 1929-73-3, 1928-43-4, 93-79-8, 2545-59-7, 116-06-3, 1646-88-4, 1646-87-3, 2032-59-9, 101-27-9, 17804-35-2, 22781-23-3, 314-40-9, 2008-41-5, 63-25-2, 10605-21-7, 1563-66-2, 55285-14-8, 101-21-3, 1982-47-4, 64-00-6, 330-54-1, 759-94-4, 101-42-8, 2164-17-2, 23422-53-9, 16655-82-6, 330-55-2, 2032-65-7, 16752-77-5, 1129-41-5, 315-18-4, 2212-67-1, 150-68-5, 555-37-3, 23135-22-0, 1114-71-2, 95-54-5, 57-47-6, 57-64-7, 2631-37-0, 122-42-9, 114-26-1, 52888-80-9, 1982-49-6, 34014-18-1 High Performance Liquid Chromatography/Thermospray/ Mass Spectrometry (HPLC/TS/MS), ultraviolet (UV)detection dyes, solid and aqueous matrices, fly ash Feb. 2007
8325 Solvent Extractable Nonvolatile Compounds by High Performance Liquid Chromatography/Particle Beam/Mass Spectrometry (HPLC/PB/MS) Determinative nonvolatiles: Benzidine, Benzoylprop ethyl, Carbaryl, o-Chlorophenyl thiourea, 3,3'-Dichlorobenzidine, 3,3'-Dimethoxybenzidine, 3,3'-Dimethoxybenzidine, Diuron, Linuron (Lorox), Monuron, Rotenone, Siduron 92-87-5, 33878-50-1, 63-25-2, 5344-82-1, 91-94-1, 119-90-4, 612-82-8, 330-54-1, 330-55-2, 150-68-5, 83-79-4, 1982-49-6 High Performance Liquid Chromatography, Particle Beam, Mass Spectrometry (HPLC/PB/MS) water, wastewater Dec. 1996
8330A Nitroaromatics and Nitramines by High Performance Liquid Chromatography (HPLC) Determinative explosives: nitroaromatics, nitramines: Octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine (HMX) Hexahydro-1,3,5-trinitro-1,3,5-triazine (RDX), 1,3,5-Trinitrobenzene (1,3,5-TNB), 1,3-Dinitrobenzene (1,3-DNB), Methyl-2,4,6-trinitrophenylnitramine (Tetryl), Nitrobenzene (NB), 2,4,6-Trinitrotoluene (2,4,6-TNT), 4-Amino-2,6-dinitrotoluene (4-Am-DNT), 2-Amino-4,6-dinitrotoluene (2-Am-DNT), 2,4-Dinitrotoluene (2,4-DNT), 2,6-Dinitrotoluene (2,6-DNT), 2-Nitrotoluene (2-NT), 3-Nitrotoluene (3-NT), 4-Nitrotoluene (4-NT) HMX: 2691-41-0, RDX: 121-82-4, 1,3,5-TNB: 99-35-4, 1,3-DNB: 99-65-0, Tetryl: 479-45-8, NB: 98-95-3, 2,4,6-TNT: 118-96-7, 4-Am-DNT: 19406-51-0, 2-Am-DNT: 35572-78-2, 2,4-DNT: 121-14-2, 2,6-DNT: 606-20-2, 2-NT: 88-72-2, 3-NT: 99-08-1, 4-NT: 99-99-0 High Performance Liquid Chromatograph (HPLC) soil, water, sediment Feb. 2007
8331 Tetrazene by Reverse Phase High Performance Liquid Chromatography (HPLC) Determinative tetrazene 31330-63-9 Reverse Phase High Performance Liquid Chromatography (HPLC) soil, water Sept. 1994
8332 Nitroglycerine by High Performance Liquid Chromatography Determinative nitrogylcerine 55-63-0 High Performance Liquid Chromatograph (HPLC) waste water, ground water, surface water Dec. 1996
8410 Gas Chromatography/Fourier Transform Infrared (GC/FT-IR) Spectrometry for Semivolatile Organics: Capillary Column Determinative semivolatile organics: Acenaphthene, Acenaphthylene, Anthracene, Benzo(a)anthracene, Benzo(a)pyrene, Benzoic acid, Bis(2-chloroethoxy)methane, Bis(2-chloroethyl) ether, Bis(2-chloro-1-methylethyl)ether, Bis(2-ethylhexyl) phthalate, 4-Bromophenyl phenyl ether, Butyl benzyl phthalate, 4-Chloroaniline, 4-Chloro-3-methylphenol, 2-Chloronaphthalene, 2-Chlorophenol, 4-Chlorophenol, 4-Chlorophenyl phenyl ether, Chrysene, Dibenzofuran, Di-n-butyl phthalate, 1,2-Dichlorobenzene, 1,3-Dichlorobenzene, 1,4-Dichlorobenzene, 2,4-Dichlorophenol, Dimethyl phthalate, Diethyl phthalate, 4,6-Dinitro-2-methylphenol, 2,4-Dinitrophenol, 2,4-Dinitrotoluene, 2,6-Dinitrotoluene, Di-n-octyl phthalate, Di-n-propyl phthalate, Fluoranthene, Fluorene, Hexachlorobenzene, 1,3-Hexachlorobutadiene, Hexachlorocyclopentadiene, Hexachloroethane, Isophorone, 2-Methylnaphthalene, 2-Methylphenol, 4-Methylphenol, Naphthalene, 2-Nitroaniline, 3-Nitroaniline, 4-Nitroaniline, Nitrobenzene, 2-Nitrophenol, 4-Nitrophenol, N-Nitrosodimethylamine, N-Nitrosodiphenylamine, N-Nitroso-di-n-propylamine, Pentachlorophenol, Phenanthrene, Phenol, Pyrene, 1,2,4-Trichlorobenzene, 2,4,5-Trichlorophenol, 2,4,6-Trichlorophenol 83-32-9, 208-96-8, 120-12-7, 56-55-3, 50-32-8, 65-85-0, 111-91-1, 111-44-4, 39638-32-9, 117-81-7, 101-55-3, 85-68-7, 106-47-8, 59-50-7, 91-58-7, 95-57-8, 106-48-9, 7005-72-3, 218-01-9, 132-64-9, 84-74-2, 95-50-1, 541-73-1, 106-46-7, 120-83-2, 131-11-3, 84-66-2, 534-52-1, 51-28-5, 121-14-2, 606-20-2, 117-84-0, 131-16-8, 206-44-0, 86-73-7, 118-74-1, 87-68-3, 77-47-4, 67-72-1, 78-59-1, 95-48-7, 106-44-5, 91-20-3, 88-74-4, 99-09-2, 100-01-6, 98-95-3, l 88-75-5, 100-02-7, 62-75-9, 86-30-9, 621-64-7, 87-86-5, 85-01-8, 108-95-2, 129-00-0, 120-82-1,l 95-95-4,88-06-2 Gas Chromatography, Fourier Transform Infrared (GC/FT-IR) Spectrometry wastewater, soils, sediments, solid wastes July 2014
8430 Analysis of Bis(2-chloroethyl) Ether and Hydrolysis Products by Direct Aqueous Injection Gas Chromatography/Fourier Transform-Infrared (GC/FT-IR) Determinative bis(2-chloroethyl)ether (BCEE), 2-Chloroethanol (CE), 2-(2-Chloroethoxy)ethanol (2CEE), Diethylene glycol (DEG), Ethylene glycol (EG) BCEE: 111-44-4, CE: 107-07-3, 2CEE: 628-89-7, DEG: 111-46-6, EG: 107-21-1 Gas Chromatography, Fourier Transform Infrared (GC/FT-IR) Spectrometry aqueous matrices July 2014
8440 Total Recoverable Petroleum Hydrocarbons by Infrared Spectrophotometry Determinative total recoverable petroleum hydrocarbons (TRPHs) NA Infrared Spectrophotometry (IR) sediment, soils, sludges Dec. 1996
8510 Colorimetric Screening Procedure for RDX and HMX in Soil Screening Hexahydro-1,3,5-trinitro-1,3,5-triazine (RDX), Octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine (HMX) 121-82-4, 2691-41-0 Colorimetric Screening soil Feb. 2007
8515 Colorimetric Screening Method for Trinitrotoluene (TNT) in Soil screening 2,4,5-Trinitrotoluene (TNT) 118-96-7 Colorimetric Screening soil Dec. 1996
8520 Continuous Measurement of Formaldehyde in Ambient Air Determinative formaldehyde 50-00-0 colorimetric analyzer ambient air Dec. 1996
8535 Screening Procedure for Total Volatile Organic Halides in Water determinative volatile organic halides (VOX): Trichloroethylene (TCE), Perchloroethylene (Tetrachloroethene) (PCE), Carbon tetrachloride, Trihalomethanes (THMs) TCE: 79-01-6, PCE: 127-18-4, 56-23-5 Colorimetric Screening water Feb. 2007
8540 Pentachlorophenol by UV-Induced Colorimetry Determinative pentachlorophenol (PCP) 87-86-5 Ultraviolet (UV)-Induced Colorimetry soil Feb. 2007
9000 Determination of Water in Waste Materials by Karl Fischer Titration determinative Water (H2O) NA Karl Fischer Titration waste Feb. 2007
9001 Determination of Water in Waste Materials by Quantitative Calcium Hydride Reaction determinative Water (H2O) NA quantitative calcium hydride reaction liquids, solids, oils, paints, soils, water/alcohol mixtures Feb. 2007
9010C Total and Amenable Cyanide: Distillation determinative Cyanide 57-12-5 reflux distillation wastes, leachates Nov. 2004
9012B Total and Amenable Cyanide (Automated Colorimetric, with Off-Line Distillation) Determinative Inorganic Cyanide 57-12-5 colorimetry wastes, leachates Nov. 2004
9013A Cyanide Extraction Procedure for Solids and Oils sample preparation soluble Cyanide 57-12-5 Extraction solids, oils, multiphase wastes July 2014
9014 Cyanide in Waters and Extracts Using Titrimetric and Manual Spectophotometric Procedures determinative non-complexed Cyanide 57-12-5 titration, colormetric drinking water, natural surface waters, domestic and industrial wastewaters, soil July 2014
9015 Metal Cyanide Complexes in Waters and Waste Extracts Using Anion Exchange Chromatography and UV Detection determinative metal cyanide complexes: Dicyanoargentate(I) ([Ag(CN)2]-), Dicyanoaurate(I) ([Au(CN)2]-), Hexacyanocolbaltate(III) ([Co(CN)6]3-), Tricyanocuprate(I) ([Cu(CN)3]2-), Hexacyanoferrate(III) ([Fe(CN)6]3-), Hexacyanoferrate(II) ([Fe(CN)6]4-), Tetracyanonickelate(II) ([Ni(CN)4]2-) With potassium as cation: 506-61-6, 554-07-4, 13963-58-1, 14264-30-3, 13746-66-2, 13943-58-3, 14220-17-8 Anion Exchange Chromatography, UV Detection water, waste July 2014
9020B Total Organic Halides (TOX) Determinative Total Organic Halides (TOX) NA microcoulometric titration drinking water, ground water Sept. 1994
9021 Purgeable Organic Halides (POX) screening Purgeable Organic Halides (POX) NA microcoulometric titration drinking water, ground water July 1992
9022 Total Organic Halides (TOX) by Neutron Activation Analysis Determinative Total Organic Halides (TOX) NA netron activation analysis aqueous samples Sept. 1986
9023 Extractable Organic Halides (EOX) in Solids Determinative Extractable Organic Halides (EOX) NA pyrolysis/ microcoulometry solid wastes, soils, suspended solids from industrial wastewater Dec. 1996
9030B Acid-Soluble and Acid-Insoluble Sulfides: Distillation sample preparation Sulfides 7704-34-9 distillation aqueous materials, solid waste, effluents Dec. 1996
9031 Extractable Sulfides sample preparation Sulfides 7704-34-9 extraction oil, solid matrices, multiphastic waste July 1992
9034 Titrimetric Procedure for Acid-Soluble and Acid-Insoluble Sulfides Determinative Sulfides 7704-34-9 titration sample extracts Dec. 1996
9035 Sulfate (Colorimetric, Automated, Chloranilate) Determinative Sulfate 14808-79-8 colorimetry ground water, drinking water, surface water, domestic waste, industrial waste Sept. 1986
9036 Sulfate (Colorimetric, Automated, Methylthymol Blue, AA II) Determinative Sulfate 14808-79-8 colorimetry ground water, drinking water, surface water, domestic waste, industrial waste Sept. 1986
9038 Sulfate (Turbidimetric) Determinative Sulfate 14808-79-8 turbidity ground water, drinking water, surface water, domestic waste, industrial waste Sept. 1986
9040C pH Electrometric Measurement Determinative pH NA electrometric pH aqueous, multiphasic waste Nov. 2004
9041A pH Paper Method Determinative pH NA litmus paper waste July 1992
9045D Soil and Waste pH Determinative pH NA electrometric pH soils, solid wastes, sludges, non-aqueous liquids Nov. 2004
9050A Specific Conductance determinative conductivity NA conductivity meter drinking water, ground water, surface water, saline waters, aqueous waste Dec. 1996
9056A Determination of Inorganic Anions by Ion Chromatography determinative inorganic anions: chloride (Cl-), fluoride (F-), bromide (Br-), nitrate (NO3-), nitrite (NO2-), phosphate (PO43-), sulfate (SO42-) 16887-00-6, 16984-48-8, 7726-95-6, 84145-82-4, 14797-65-0, 98059-61-6, 18785-72-3 ion chromatography drinking water, wastewater, aqueous extracts of solids, collection solutions from bomb combustion of solid waste Feb. 2007
9057 Determination of Chloride from HCl/Cl2 Emission Sampling Train (Methods 0050 and 0051) by Anion Chromatography determinative chloride (Cl-) 16887-00-6 ion chromatography stack gas emission samples Dec. 1996
9060A Total Organic Carbon Determinative Total Organic Carbon (TOC) NA carbonaceous analyzer ground water, surface water, saline waters, domestic waste, industrial waste Nov. 2004
9065 Phenolics (Spectrophotometric, Manual 4-AAP with Distillation) Determinative phenolics NA colorimetry ground water, surface water, saline waters, domestic waste, industrial waste Sept. 1986
9066 Phenolics (Colorimetric, Automated 4-AAP with Distillation) Determinative phenolics NA colorimetry ground water, drinking water, surface water, saline waters Sept. 1986
9067 Phenolics (Spectrophotometric, MBTH with Distillation) Determinative phenolics NA colorimetry drinking water, ground water, surface water, saline waters, domestic waste, industrial waste Sept. 1986
9070A N-Hexane Extractable Material (HEM; Oil and Grease) and Silica Gel Treated N-Hexane Extractable Material (SGT-HEM; Non-polar Material) By Extraction and Gravimetry Determinative N-Hexane Extractable Material (HEM)   extraction and gravimetry surface water, saline waters, industrial aqueous waste, domestic aqueous waste Nov. 2004
9071B n-Hexane Extractable Material (HEM) for Sludge, Sediment, and Solid Samples Determinative oil and grease NA Soxhlet extraction sludge, sediment, solids Apr. 1998
9074 Turbidimetric Screening Method for Total Recoverable Petroleum Hydrocarbons in Soil screening petroleum hydrocarbons NA Turbidity soil Feb. 2007
9075 Test Method for Total Chlorine in New and Used Petroleum Products by X-Ray Fluorescence Spectrometry (XRF) Determinative chlorine (Cl2) 16887-00-6 X-Ray Fluorescence Spectrometry (XRF) new & used oils, fuels, crankcase oil, hydraulic oil, diesel oil, lubricating oil, fuel oils, kerosene Sept. 1994
9076 Test Method for Total Chlorine in New and Used Petroleum Products by Oxidative Combustion and Microcoulometry Determinative chlorine (Cl2) 16887-00-6 oxidative combustion and microcoulometry new & used oils, fuels, crankcase oil, hydraulic oil, diesel oil, lubricating oil, fuel oils, kerosene Sept. 1994
9077 Test Methods for Total Chlorine in New and Used Petroleum Products (Field Test Kit Methods) Determinative chlorine (Cl2) 16887-00-6 field kit new or used petroleum products Sept. 1994
9078 Screening Test Method for Polychlorinated Biphenyls in Soil screening Polychlorinated Biphenyls (PCBs) 1336-36-3 field kit soil, sand, gravel, loam, clay, sediment Dec. 1996
9079 Screening Test Method for Polychlorinated Biphenyls in Transformer Oil Screening Polychlorinated Biphenyls (PCBs) 1336-36-3 field kit transformer oil, electrical insulating fluids Dec. 1996
9080 Cation-Exchange Capacity of Soils (Ammonium Acetate) Determinative cation-exchange capacity (CEC) NA Ammonium Acetate exchange soil Sept. 1986
9081 Cation-Exchange Capacity of Soils (Sodium Acetate) Determinative cation-exchange capacity (CEC) NA sodium actetate exchange soil Sept. 1986
9090A Compatibility Test for Wastes and Membrane Liners Determinative compatibility with membrane liners NA long-term immersion waste destined for surface impoundment, waste pile, or landfill July 1992
9095B Paint Filter Liquids Test Determinative free liquids NA filtration waste Nov. 2004
9096 Liquid Release Test (LRT) Procedure Determinative liquid release NA overburden pressure test waste destined for landfill Sept. 1994
9100 Saturated Hydraulic Conductivity, Saturated Leachate Conductivity, and Intrinsic Permeability determinative conductivity, permeability NA constant head methods, falling head methods, modified compaction permeameter method, triaxial cell method, pressure-chamber permeameter method, single bore hole methods, piezometer methods earth materials, leachate, soil liners Sept. 1986
9131 Total Coliform: Multiple Tube Fermentation Technique determinative total Coliform NA multiple tube fermentation ground water, surface water Sept. 1986
9132 Total Coliform: Membrane-Filter Technique determinative total Coliform NA membrane-filter wastewater, ground water Sept. 1986
9210A Potentiometric Determination of Nitrate in Aqueous Samples with Ion-Selective Electrode determinative Nitrate (NO3-) 14797-55-8 ion-selective electrode drinking water, natural surface water, groundwater, domestic & industrial wastewater, soil extracts, aqueous extracts Feb. 2007
9211 Potentiometric Determination of Bromide in Aqueous Samples with Ion-Selective Electrode determinative Bromide (Br-) 7726-95-6 ion-selective electrode drinking water, natural surface water, groundwater, domestic & industrial wastewater, soil extracts Dec. 1996
9212 Potentiometric Determination of Chloride in Aqueous Samples with Ion-Selective Electrode determinative Chloride (Cl-) 16887-00-6 ion-selective electrode drinking water, natural surface water, groundwater, domestic & industrial wastewater, soil extracts Dec. 1996
9213 Potentiometric Determination of Cyanide in Aqueous Samples and Distillates with Ion-Selective Electrode determinative Cyanide (CN-) 57-12-5 ion-selective electrode drinking water, natural surface water, groundwater, domestic & industrial wastewater, soil extracts Dec. 1996
9214 Potentiometric Determination of Fluoride in Aqueous Samples with Ion-Selective Electrode determinative Fluoride (F-) 16984-48-8 ion-selective electrode drinking water, natural surface water, groundwater, domestic & industrial wastewater, soil extracts Dec. 1996
9215 Potentiometric Determination of Sulfide in Aqueous Samples and Distillates with Ion-Selective Electrode determinative Sulfide (S2-) 18496-25-8 ion-selective electrode distilled samples Dec. 1996
9216 Potentiometric Determination of Nitrite in Aqueous Samples with Ion-Selective Electrode determinative Nitrite (NO2-) 14797-65-0 ion-selective electrode drinking water, wastewater, reagent waters Feb. 2007
9250 Chloride (Colorimetric, Automated Ferricyanide AAI) determinative Chloride (Cl-) 16887-00-6 Colorimetric ground water, drinking water, surface water, saline waters Sept. 1986
9251 Chloride (Colorimetric, Automated Ferricyanide AAII) determinative Chloride (Cl-) 16887-00-6 Colorimetric ground water, drinking water, surface water, saline waters, domestic & industrial waste Sept. 1986
9253 Chloride (Titrimetric, Silver Nitrate) determinative Chloride (Cl-) 16887-00-6 Titrimetric oxygen bomb combustates, water Sept. 1994
9310 Gross Alpha and Gross Beta sampling gross alpha, gross beta NA particle activity measurement surface water, ground waters Sept. 1986
9315 Alpha-Emitting Radium Isotopes sampling radium-223, radium-224, radium-226 444811-40-9, 13233-32-4,, 7440-14-4 coprecipitation surface water, ground water Sept. 1986
9320 Radium-228 determinative radium-228, radium-226 15262-20-1, 7440-14-4 Coprecipitation groundwater July 2014

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