Regulatory Text: 
Louisiana Administrative Code, Title 33 ENVIRONMENTAL QUALITY, Part III Air (LAC 33:III)

Chapter 15. Emission Standards for Sulfur Dioxide

Section 1503.D.2. TABLE 4. Emissions--Methods of Contaminant Measurement
As adopted in the Louisiana Register December 20, 1996 (LR 22:1212,p 2 to 5) (AQ145)
Approved/As approved by EPA July 5, 2011 (76 FR 38977) effective August 4, 2011 (LAd34) LA021.
Regulations.gov docket EPA-R06-OAR-2007-0924

Although not listed in the July 5, 2011 (76 FR 38977) Federal Register amendatory language (see page 76 FR 38982), this Table 4 assumes that EPA approved revisions to Table 4 adopted in the Louisiana Register December 20, 1996 (LR 22:1212,p 2 to 5) (AQ145) in the July 5, 2011 Federal Register action.  This is in order to be consistent with other revisions adopted in the December 20, 1996 Louisiana Register approved by EPA in the July 5, 2011 Federal Register and to be consistent with Table 4 in the current Louisiana Air Quality Control Regulations. 


-------------     ----------------------------------------
Emission                 Analytical Method
-------------     ----------------------------------------

Particulate       
                  1) Methods 1, 2, 3, 4, 5 (40 CFR part 60, 
                     appendix A, as incorporated by reference 
                     at LAC 33:III.3003) or §60.8 of 40 CFR 
                     part 60 as incorporated by reference at 
                     LAC 33:III.3003. 
                     


Sulfur Oxides
                  1) Seidman, Analytical Chemistry Volume
                     30, page 1680 (1958),"Determination
                     of Sulfur Oxides in Stack Gases."
                  2) Shell Development Company method for
                     the Determination of Sulfur Dioxide
                     and Sulfur Trioxide PHS 999 AP-13
                     Appendix B, pages 85-87, "Atmospheric
                     Emissions Sulfuric Acid
                     Manufacturing Processes."
                  3) Reich Test for Sulfur Dioxide,
                     "Atmospheric Emissions from Sulfuric
                     Acid Manufacturing Process" PHS 999
                     AP-13 Appendix B, pages 76-80.
                  4) The Modified Monsanto Company Method,
                     "Atmospheric Emissions from Sulfuric
                     Acid Manufacturing Process" PHS 999
                     AP-13, Appendix B, pages 61-67.
                  5) Test Methods 1, 2, 3, 4, 6, and 8 (40 CFR part 60, 
                     appendix A, as incorporated by reference at 
                     LAC 33:III.3003) or §60.8 of 40 CFR part 60 
                     as incorporated by reference at LAC 33:III.3003.


Oxides of Nitrogen          
                  1) Test Methods 1, 2, 3, 4, and 7 (40 CFR part 60, 
                     appendix A, as incorporated by reference at 
                     LAC 33:III.3003) or §60.8 of 40 CFR part 60 as 
                     incorporated by reference at LAC 33:III.3003.


Visible Emissions 
                  1) Method 9 (40 CFR part 60, appendix A, 
                     as incorporated by reference at LAC 33:III.3003).
                  2) Method 22 (40 CFR part 60, appendix A, 
                     as incorporated by reference at LAC 33:III.3003).

Total Fluoride    
                  1) Methods 1, 2, 13A, and 13B (40 CFR part 60,
                     appendix A, as incorporated by reference at 
                     LAC 33:III.3003).

Total Reduced Sulfur (TRS)
                  1) Method 16 (40 CFR part 60, appendix A, or §60.8 
                     of 40 CFR part 60 as incorporated by reference 
                     at LAC 33:III.3003).
                  2) Coulometric titration by method
                     specified in NCASI Atmospheric
                     Quality Improvement Technical
                     Bulletin Number 91. (January 1978)

Sulfuric Acid Mist
                  1) Test methods 1, 2, 3, 4, 6, and 8 (40 CFR part 60, 
                     appendix A, or §60.8 of 40 CFR part 60 as 
                     incorporated by reference at LAC 33:III.3003.)